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3 method specifications of the method testpb.mth – Metrohm 746 VA Trace Analyzer User Manual

Page 95

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4 Introduction to the operation

746 VA Trace Analyzer / 747 VA Stand

4-10

The header of dialog page "METHODS" contains details of the number of stored
methods and the available storage space. This is followed by the names of all stored
methods displayed in 4 columns.
You obtain a different type of display if you press the softkeyy
. In
addition to the name of the method, its content (method title) and memory requirements
are shown.
You will find further information regarding the dialog page "METHODS" in section 5.4.1.

3

Selection of the method

TESTPb.mth

Use the cursor keys to select the method

TESTPb.mth

, which then

becomes black-backed.

4

Copying the method

TESTPb.mth to the working storage

Press the softkey

. The softkey bar changes and presents the

destinations for copying the selected method.

Press the softkey

. The method

TESTPb.mth

is

copied to the working storage.

4.2.3

Method specifications of the method

TESTPb.mth

In this section the 5 dialog pages of the group "Method Specifications" associated

with the loaded method

TESTPb.mth

will be explained in detail. If you are interested

only in a rapid lead measurement, you can proceed directly to section 4.2.4.

1

Switch to dialog page "OPERATION SEQUENCE"

Press the yellow key. The dialog page "OPERATION

SEQUENCE" appears with the main program for the lead determination:

Method: TESTPb .mth OPERATION SEQUENCE

Title : Pb determination in ion standard solution

Instructions t/s Main parameters Auxiliary parameters

ДДДДДДДДДДДДД

ДДДДДДДДДДДДД ДДДДД

ДДДДД ДДДДДДДДДДДДДДДДДДДДДДДДД

ДДДДДДДДДДДДДДДДДДДДДДДДД

ДДДДДДДДДДДДДДДДДДДДДДДДД

ДДДДДДДДДДДДДДДДДДДДДДДДД

1 DOS/M V.added 20.500 mL

2 REM 20 mL distilled water + 0.5 mL KCl 3 mol/L

3 SMPL/M V.fraction mL V.total L

4 REM 100 uL Pb ion standard 1 g/L

5 PURGE

6 STIR 300.0 Rot.speed 2000 /min

7 (ADD

8 PURGE

9 STIR 30.0 Rot.speed 2000 /min

10 ØPURGE

11 ØSTIR 5.0

12 (REP

13 SEGMENT Segm.name SegPb

14 REP)2

15 ADD>M Soln.name PbStd V.add 0.100 mL

16 ADD)2

17 END

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column

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line

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instr.

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instr.

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