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291 smpl>m, O, s, M, a – Metrohm 746 VA Trace Analyzer User Manual

Page 442: Smpl

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5.7.3 Alphabetical instruction list

746 VA Trace Analyzer / 747 VA Stand

5-291

SMPL>M

Page:

O, S

Stand:

M, A

Abbreviation:

SMPL>

Instructions t/s Main parameters Auxiliary parameters

––––––––––––– ––––– ––––––––––––––––––––––––– –––––––––––––––––––––––––

## .. SMPL>M ..... V.fraction ........mL V.total .........L

Function

Add sample volume to the measuring vessel (MEAS).

Parameter

Range; Default value / Meaning

V.fraction

0.010...50.000 mL; -

Fractional volume

With diluted samples, here the volume fraction of the total volume

V.total

which is added to the sample vessel must be entered. The

following condition holds:

V.fraction

≤≤ V.total

V.total

0.10 mL...100000 L; -

Total volume

With diluted samples, here the total volume of sample and dilution
solution must be entered. The following condition holds:

V.total

≥≥ V.fraction

Description

The

SMPL>M

instruction is used for the manual or automatic addition of

the sample volume to the measuring vessel (MEAS) on the 747 VA
Stand:

In manual addition or addition with the 6.5611.010 Pipet-
ting equipment, the prompt

SMPL "V.sample" > M

for

manual addition of the sample volume

V.sample

appears

in the program run.

In automatic addition with the 695 Autosampler, the sam-
ple volume is transferred from the sample vessel on the
sample rack defined on the 1

st

sample data line to the

measuring vessel.

With undiluted samples (

V.fraction

and

V.total

blank), the sample

volume is given either by

S0

(on entry of

S0

as a volume) or by

S0/S2

(on entry of

S0

as a weight,

S2

is the density in g/mL).

With diluted samples (

V.fraction > 0

and

V.total

≥≥ V.fraction

), the

sample volume is given by

V.fraction

, irrespective of the entry of

S0

.

You will find further details on the sample size in the description of the
parameter

Sample size/S0

in section 5.4.4.

see also

SMPL/M, SMPL/F