246 meas, O, s, M, a – Metrohm 746 VA Trace Analyzer User Manual
Page 397
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5.7 Program instructions
746 VA Trace Analyzer / 747 VA Stand
5-246
MEAS
Page:
O, S
Stand:
M, A
Abbreviation:
M
Instructions t/s Main parameters Auxiliary parameters
––––––––––––– ––––– ––––––––––––––––––––––––– –––––––––––––––––––––––––
## .. MEAS ..... U.meas ........mV
Function
Application of a constant voltage to the electrodes and measurement of
the current without measured value storage.
Application
The
MEAS
instruction is primarily used together with the HMDE or RDE
for electrochemical enrichment in stripping voltammetry.
Parameter
Range; Default value / Meaning
U.meas
-3000...3000 mV; -
Measurement voltage
The voltage entered here is applied to the electrodes. This voltage
remains in force even after the line time has elapsed until a SWEEP
instruction follows or until it is switched off by
ØMEAS
or
END
in the main
program on the "OP.SEQUENCE" page.
Description
The
MEAS
instruction applies the voltage defined in the
U.meas
para-
meter to the electrode. At the same time, the current measurement is
started in accordance with the parameters defined in the measurement
mode. The duration of the measurement is defined with the line time.
During an ongoing measurement with
MEAS
, the current measured
values for voltage and current are displayed in the measurement window
on the "MONITORING" page (see section 5.5.1).
Comments
•
The electrode type must be defined before the
MEAS
instruction.
Admissible are
DME
,
SMDE
,
HMDE
or
RDE
.
•
The measurement mode must be defined before the
MEAS
instruc-
tion. Admissible are
DCTMODE
,
DPMODE
,
AC1MODE
,
AC2MODE
,
SQWMODE
,
CYCMODE
or
PSAMODE
.
•
If the measured values in measurement of the current should be
plotted, the
TSWEEP
instruction must be used in place of the
MEAS
instruction. However, this must not be in the same segment as the
measurement sweep.
•
If the measurement voltage
U.meas
should not be switched off at the
end of the program, enter a suitable standby voltage
U.standby
in a
ØMEAS
instruction.