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Metrohm 746 VA Trace Analyzer User Manual

Page 518

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7.3 Error messages

746 VA Trace Analyzer / 747 VA Stand

7-19

Error message

Meaning/Causes

Rectification

Exit

MEASURE - ERROR 30:
Missing voltage value

Voltage value in sweep is not

defined (

U.end

,

U.start

or

U.meas

)

Enter voltage values in the

SWEEP

instruction

E/S

MEASURE - ERROR 31:
Illegal replication

Inadmissible replication in

conjunction with measurement

mode

CYCMODE

Clear replication

(REP...REP)n

E/C

MEASURE - ERROR 32:
Missing mass concentra-
tion (SOLUTIONS)

The mass concentration

Mass

conc.

is missing on the

”SOLUTIONS” page

Enter mass concentration

Mass conc.

on the ”SOLUTIONS” page

E/S

MEASURE - ERROR 33:
Standard addition with
different solutions

In the standard addition,

spiking was not performed with

the same standard addition

solution (different sequence in

conjunction with CASE instruc-

tions)

Check programming of the CASE

instructions

E/C

MEASURE - ERROR 34:
from this page
impossible

Program start from the

”STAND” and ”CURVES”

pages not possible

Switch to the ”MONITORING” page and

press

E/C

MEASURE - ERROR 35:
Variation parameter out
of range

The range limits of the varied

parameter were exceeded

Change

Delta

parameter in the

VARNI

instruction or number of variation

cycles

E/S

MEASURE - ERROR 36:
Missing solution

An entry is not available for

every substance on the

”SOLUTIONS” page

Missing or wrong substance

name

Enter solution for every substance on

the ”SOLUTIONS” page (also with

mixed solutions)

Check substance name on the

”SOLUTIONS,” SUBSTANCES” and

”OP.SEQUENCE” or ”SEGMENTS”

pages

E/S

MEASURE - ERROR 37:
Measurement data
inconsistent

The experimental data are

incomplete, e.g. owing to

instrument being switched off

during an ongoing measure-

ment

Restart measurement

E/C

MEASURE - ERROR 38:
Too small volume in
FEED or AUX

Insufficient solution for the

desired transfer instruction in

the sample vessel FEED or in

the auxiliary vessel AUX on the

695 Autosampler

Lower volume

V.add

for transfer

instruction

E/S

MEASURE - ERROR 39:
Incomplete calibration

The calibration has not been

run to completion

Restart calibration

E/S

MEASURE - ERROR 40:
PREP demands Auto.batch
= on

PREP loops are admissible only

when

Auto.batch = on

is set

Set

Auto.batch = on

on the

”MONITORING” page

E/C

MEASURE - ERROR 41:
Different V.total in
SMPL

On entry of several SMPL

instructions,

V.total

must be

identical in all cases

Set

V.total

the same for all SMPL

instructions on the ”OP.SEQUENCE” or

”SEGMENTS” page

E/C

MONITORING - ERROR 1:
Can not start as busy
measuring

The called-up function can not

be executed as a measurement

is running

Wait until measurement ended

E/C

MONITORING - ERROR 2:
Live display only when
BUSY

Display of the live curve not

possible as no measurement is

running

Start measurement

E

OP.SEQ. - ERROR 1:
Missing END instruction

Missing

END

instruction

Append

END

instruction to end of

program on the ”OP.SEQUENCE” page

Esc

OP.SEQ. - ERROR 2:
Nesting violation: line
##

Error in the nesting of instruc-

tions with brackets

Check program on the ”OP.SE-

QUENCE” page for correct use of

instructions with brackets and correct if

necessary

Esc