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Metrohm 746 VA Trace Analyzer User Manual

Page 179

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5.3 Set Up

746 VA Trace Analyzer / 747 VA Stand

5-28

Softkeys

Meaning

Prime

tube

Fill transfer tubing

By pressing this softkey the transfer tubing is automatically refilled
with hydraulic solution. This may be necessary in two cases:

For filling empty transfer tubing.

For expelling interfering air bubbles.

For further details, please see the 695 Instructions for use.

Cond.

tube

Clean transfer tubing

Contamination of the transfer tubing is normally shown by breaking up
of the air bubbles used to separate the solutions, i.e. they are no
longer durable. In this case, an attempt can be made to free the
transfer tubing from contamination using a cleaning solution, prefera-
bly Javelle water (hypochlorite solution). Proceed as follows:

Press

. The transfer needle is moved to a posi-

tion in front of the 747 VA Stand, at the same time the prompt

Put solution on cond. position

appears.

Position a vessel containing sufficient Javelle water below the
transfer needle.

Press . The transfer tubing is filled with Javelle
water. After a wait of 1 min., the transfer needle is moved to
the waste position and the solution expelled

Repeat the entire procedure once more.

For further details, please see the 695 Instructions for use.

Rinsing

Dosinos

Switch to Rinsing Dosinos

The measuring vessel at the 747 VA Stand are rinsed by means of two
700 Dosinos with 50 mL dosing units screwed to supply containers,
one of which adds the rinsing solution while the other siphons off any
wash solutions into the waste container. This softkey is used to switch
to the manual operation of the two rinsing Dosinos. The following
functions are available:

Rinse

meas.v.

Rinse measuring vessel

After this softkey has been pressed, the measuring vessel is auto-
matically rinsed as follows:

The solution in the measuring vessel is siphoned off.

The measuring vessel is filled with the volume of rinsing solu-
tion defined as

V.rinse

.

The rinsing solution is siphoned off.

The measuring vessel is filled with the volume of rinsing solu-
tion defined as

V.standby

(conditioning solution).

Prime

Dosinos

Initialize rinsing Dosinos

The burette cylinders of the rinsing Dosinos and all connecting tubing
up to the measuring vessel and the wash station are automatically
filled with rinsing solution.

Empty

Dosinos

Empty Dosinos

The burette cylinders of the rinsing Dosinos, the wash station and all
connecting tubing up to the measuring vessel and the wash station
are emptied.