Metrohm 746 VA Trace Analyzer - Manual (Page 366)

5.7.3 Alphabetical instruction list
746 VA Trace Analyzer / 747 VA Stand
5-215
CSOLN/M Page: O, S Stand: M Abbreviation: CSOLN/M
Instructions t/s Main parameters Auxiliary parameters
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## .. CSOLN/M ..... solution added into MEAS
Function Calibration solution is already in the measuring vessel (MEAS).
Description The CSOLN/M instruction is used for the recording of calibration curves
with the techniques cal.crv. and int.std. with the manual 747 VA
Stand. Within a CAL loop, it defines that the calibration solution is already
located in the measuring vessel (MEAS).
Comments • The CSOLN/M instruction can not be used in operation with the 695
Autosampler.
• In contrast to the CSOLN>M instruction, with CSOLN/M no prompt to
add the calibration solution appears during the program run. As a
new calibration solution must be used for every concentration, within
the CAL loop it is mandatory to insert a
RINSE instruction which
resets the volume bookkeeping in the measuring vessel to 0 (see
also
RINSE). To ensure that the prompt Change measuring vessel
to change the solution appears, its parameter Cycles > 0 must be
set.
• The number of calibration solutions is defined with n in the CAL)n
instruction. A valid mass concentration Mass conc. must be entered
on the "SUBSTANCES/Calibration" page for each of these solutions.
• In the V0.CSoln parameter on the "SUBSTANCES/Calibration" page,
the volume valid for all calibration solutions that have been added to
the measuring vessel (MEAS) must be entered.
• If work is performed with Auto.samples = on , on the "SAMPLES"
page sample data lines must be entered in immediate succession for
all n calibration solutions with the following holding for their parame-
ters:
S1...S3 Sample identifications (only entries of the last
calibration solution are used and stored)
Method.call Name of the method + .C
(for mode calibration)
Sample Size/S0 Entry of an asterisk *
(value not used, but field must not be blank)
• For permanent storage of the coefficients of the calibration curve
determined in the recording of the calibration solutions, the method
must then be copied from the working storage to the method memory
(this occurs automatically with
Auto.batch = on ).