beautypg.com

Metrohm 746 VA Trace Analyzer User Manual

Page 439

background image

5.7 Program instructions

746 VA Trace Analyzer / 747 VA Stand

5-288

Comments

Within a program, the SMDE is not switched off until an

ØMEAS

instruction or selection of a different electrode type (

DME

,

HMDE

or

RDE

). The SMDE is also switched off by

END

in the main program on

the "OP.SEQUENCE" page, but not by

END

in the segment.

The SMDE can be used for the following measurement modes and
sweeps:

DCTMODE

with

SWEEP

and

SSWEEP

,

DPMODE

with

SWEEP

and

FSWEEP

,

SQWMODE

with

SWEEP

and

FSWEEP

,

AC1MODE

with

SWEEP

and

AC2MODE

with

SWEEP

.

The following are not compatible with the SMDE:

CYCMODE

with

(CSWEEP

,

PSAMODE

with

PSWEEP

as well as

TSWEEP

.

An advantage of the SMDE compared with the DME is its greater
sensitivity as the electrode surface and hence the baseline remains
constant during the measurement. Further, less mercury is needed.
On the other hand, the MME capillary is subjected to greater me-
chanical stress than in the DME case.

A disadvantage of the SMDE compared with the HMDE is the higher
mercury consumption, in addition the MME is subjected to greater
mechanical stress.

see also

DME, HMDE, RDE