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Metrohm 746 VA Trace Analyzer User Manual

Page 70

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3.10 Connection of 700 Dosinos

746 VA Trace Analyzer / 747 VA Stand

3-43

3.10.3 Tubing connection for addition of auxiliary solutions

The 4-way microtip 47

47 is not suited for the addition of auxiliary solutions in the mL-

range into the measuring vessel of the 747 VA Stand. For the addition of a first aux-

iliary solution we recommend the use of the following accessories:

• 1 ×× 6.1819.000 PTFE tube, length L = 77 mm, i.d. = 0.8 mm

• 2 ×× 6.1805.100 FEP tubing, length L = 40 cm, i.d. = 2 mm

• 1 ×× 6.1808.000 Coupling

To install these accessories and ready the 700 Dosino for automatic dispensing,

proceed as follows:

1 Mount Dosing unit on 700 Dosino

Procedure, see section 2.2 of 700 Instructions for Use.

2 Insert PTFE tube in 747 VA Stand

Cut 6.1819.000 PTFE tube (optionally available) to a length of ca. 30 mm

(the tip of the tube should never be immersed into the solution).

Remove dummy stopper 42

42 and insert PTFE tube from above in the

opening 78

78 of the measuring head 41

41 (see Fig. 9).

3 Connect FEP tubing to Dosing unit

Screw 6.1805.100 FEP tubing (optionally available) into opening 78

78.

Screw a 1808.000 Coupling (accessory of 747 VA Stand) to the other end

of the 6.1805.100 FEP tubing and insert this in a slot of the tubing holder

at the rear of the 747 VA Stand.

Screw the 6.1805.100 FEP tubing (accessory of Dosing unit) onto con-

nection 1 of the Dosing unit.

Screw the other end of the 6.1805.100 FEP tubing attached to the Dosing

unit to the 6.1808.000 Coupling just inserted in the tubing holder of the

747 VA Stand.

4 Initialize Dosino(s)

Switch on 746 VA Trace Analyzer using the mains switch 11

11.

Select dialog page "DOSIMATS".

Set parameter

V.init

to

0.00 mL

.

Set parameter

V.tube in

to

0.7 mL

.

Set parameter

V.tube out

to

3.0 mL

.

Press softkey

for initializing all attached Dosinos or select

desired Dosino with the cursor keys and press softkey

:

The cylinder is filled and excess solution is expelled to the measuring

vessel. With standard accessories, all tubings to the measuring vessel will

have been filled at the end of the initializing procedure.