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Metrohm 746 VA Trace Analyzer User Manual

Page 139

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4 Introduction to the operation

746 VA Trace Analyzer / 747 VA Stand

4-54

9

Printout of reports and curves

On completion of the program, the reports and curves entered on the

"DOCUMENTATION" page are put out on the printer:

================== METROHM 746 VA TRACE ANALYZER (5.746.0101) ==================

Determ. : 12161627 User: Date: 1996-12-16

Modified : no Run : 5 Time: 16:27:07

Sample table: -

--------------------------------------------------------------------------------

Pos. Ident.1/S1 Ident.2/S2 Ident.3/S3 Method.call Sample size/S0

Drink water 10 mL

--------------------------------------------------------------------------------

Method : INTSTD

Title : Pb determination with calibration curve

Remark1 :

Remark2 :

--------------------------------------------------------------------------------

Substance : Pb Comments

Mass conc.: 13.02 ug/L Mass : 130.2 ng ——————————————————

MC.dev. : 0.603 ug/L (4.63%) Add.mass : - dev. estimated

Cal.dev. : 0.326 ug/L (2.5%) V0.sample: 10 mL

VR U/mV I/nA I.mean Std.dev. I.delta Comments

——— ————— —————— —————— ——————— ——————— ——————————————————

00 -409 17.66 17.74 0.1623

01 -409 17.92

02 -409 17.63

Substance : CdRef Comments

Mass conc.: - Mass : - ——————————————————

MC.dev. : - Add.mass : -

Cal.dev. : - V0.sample: -

VR U/mV I/nA I.mean Std.dev. I.delta Comments

——— ————— —————— —————— ——————— ——————— ——————————————————

00 -583 23.78 23.90 0.1073

01 -583 24.00

02 -584 23.92

Substance Techn. Y.reg/offset Slope Nonlin. Mean.deviat.

————————— ———————— ———————————— —————————— —————————— ————————————

Pb int.std. 0.5699 0.03553

CdRef int.std.

C# Workg.com.var Remark

—— ————————————— ————————————————

Final results +/- Res.dev. % Comments

————————————————————————————————— ————————————————— ——————————————————

Pb = 13.02 ug/L 0.603 4.63 see Evaluations

The full report

Full report

contains not only the usual header (see

section 4.2.6), but also the following important sections:

1

Data for substance

Results of peak evaluations and result for Pb mass

evaluation of Pb

concentration.

2

Data for substance

Only the substance name

CdRef is given, the

evaluation of Cd

other parameters remain blank as they are not
calculated when the calibration curve is recorded.

3

Data for calibration

The proportionality factor determined from the
calibration curve is given.

4

Final results

Final result with formula calculation.

3

1

2

4