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4 introduction to the operation – Metrohm 746 VA Trace Analyzer User Manual

Page 135

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4 Introduction to the operation

746 VA Trace Analyzer / 747 VA Stand

4-50

================== METROHM 746 VA TRACE ANALYZER (5.746.0101) ==================

Determ. : 12161422 User: Date: 1996-12-16

Modified : no Run : 4 Time: 14:22:33

Sample table: -

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Pos. Ident.1/S1 Ident.2/S2 Ident.3/S3 Method.call Sample size/S0

10 mL

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Method : INTSTD

Title : Pb determination with internal standard (Cd)

Remark1 :

Remark2 :

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Substance : Pb Comments

Mass conc.: - Mass : - ——————————————————

MC.dev. : - Add.mass : -

Cal.dev. : - V0.sample: -

VR U/mV I/nA I.mean Std.dev. I.delta Comments

——— ————— —————— —————— ——————— ——————— ——————————————————

00 -407 3.664 3.721 0.0523

01 -408 3.767

02 -408 3.732

10 -408 7.289 7.134 0.1342 3.413

11 -407 7.056

12 -407 7.057

20 -408 13.30 14.14 1.095 7.010

21 -408 15.38

22 -408 13.75

30 -408 28.18 27.12 0.9354 12.97

31 -408 26.77

32 -408 26.41

Substance : CdRef Comments

Mass conc.: - Mass : - ——————————————————

MC.dev. : - Add.mass : -

Cal.dev. : - V0.sample: -

VR U/mV I/nA I.mean Std.dev. I.delta Comments

——— ————— —————— —————— ——————— ——————— ——————————————————

00 -583 24.47 24.73 0.2262

01 -583 24.89

02 -583 24.82

10 -583 25.55 25.04 0.4501 0.3084

11 -583 24.73

12 -583 24.82

20 -582 22.60 23.77 1.480 -1.268

21 -582 25.43

22 -583 23.27

30 -583 25.53 24.80 0.6384 1.029

31 -583 24.51

32 -583 24.35

Substance Techn. Y.reg/offset Slope Nonlin. Mean deviat.

————————— ———————— ———————————— —————————— —————————— ————————————

Pb int.std. 0.5699 0.03553

CdRef int.std.

C# Workg.com.var Remark

—— ————————————— ————————————————

Final results +/- Res.dev. % Comments

————————————————————————————————— ————————————————— ——————————————————

Pb = 0.0000 g/L 0.000 - var. not found

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