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Metrohm 746 VA Trace Analyzer User Manual

Page 466

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6.2 Preparations before start of a determination

746 VA Trace Analyzer / 747 VA Stand

6-3

SEGMENTS

This dialog page is used to define the measured value recording using pro-

gram instructions and their parameters (see section 5.7.3). The most impor-

tant instructions concern selection of the electrode, the measurement mode

and the sweep:

Electrode

DME

,

SMDE

,

HMDE

,

RDE

Measurement

DCTMODE

,

DPMODE

,

SQWMODE

,

AC1MODE

,

mode

AC2MODE

,

PSAMODE

,

CYCMODE

Sweep

SWEEP

,

SSWEEP

,

FSWEEP

,

TSWEEP

,

PSWEEP

,

(CSWEEP...RAMP...CSWEEP)

A total of 8 different segments can be programmed to which the desired sub-

stances can be assigned. The segments are distinguished by their name.

SUBSTANCES

On this dialog page maximum 8 different substances with their specific pa-

rameters can be defined. Each desired substance requires the following en-

tries:

Substance name
Assignment to a segment

(without assignment, there is no substance evaluation)

– Parameters for substance recognition (Recognition)
– Parameters for baseline calculation (Baseline)
– Definition of the evaluation quantity (Evaluation)
– Parameters for curve display and plot (Display/Plot)
– Parameters for calibration

(standard addition, calibration curve or internal standard)

CALCULATION

On this dialog page freely selectable calculation formulae for further calcula-

tion of the standard results obtained in the evaluation to produce the desired

final results can be entered.

DOCUMENTATION

This dialog page is used for definition of the automatic output of reports and

curves on the built-in printer or the printer connected at the parallel or RS232

interface. Further, there is a possibility to enter a detailed comment on the

method.