Metrohm tiamo 1.0 Manual User Manual
Page 397
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Commands
373
Control
(only visible for
Titration rate
=
user
)
Dynamics pH
0.001 ... [ 2.000 (slow) ] ... [ 2.000 (optimal) ] ... [ 0.500 (fast) ] ... 20.000, off
(Titrando),
0.01 ... [ 2.00 (slow) ] ... [ 2.00 (optimal) ] ... [ 0.50 (fast) ] ... 20.00, off
(Titrino)
Dynamics defines the measured value range before the given endpoint.
This parameter has an important influence on the titration rate and with it on
the accuracy. Within the control range the steps which are added are con-
trolled by the
Min. rate
. The nearer the endpoint the slower the dosing takes
place until the
Min. rate
has been reached. Outside the range the dosing
takes place with
Max. rate
) (see Control range).
Max. rate
0.01 ... [ 1.00 (slow) ] ... [ 10.00 (optimal) ] ... 166.00 mL/min, [ maximal (fast) ]
(Titrando)
0.01 ... [ 1.00 (slow) ] ... [ 10.00 (optimal) ] ... 150.00 mL/min, [ maximal (fast) ]
(Titrino)
Speed of addition outside the control range. The maximum dosing speed
depends on the cylinder volume of the exchange unit or dosing unit used.
Min. rate
0.01 ... [ 5.00 (slow)] ... [ 25.00 (optimal) ] ... [ 50.00 (fast) ] ... 9999.00 µL/min
Speed of addition at the start and finish of the titration. The slower the
minimum rate that is selected, the slower the titration and the higher the ac-
curacy.
Stop criterion
Stop criterion
[ drift ], time, off
The titration stops when the endpoint has been reached and the stop crite-
rion has been fulfilled. The titration can be stopped when a particular
drift
has been achieved or after a preset
time
. If no stop criterion has been se-
lected the titration will not be stopped.
Note
The Stop conditions will always stop the titration even if the stop criterion has not
been fulfilled or has been turned off.
Stop drift
1 ... [ 20 ] ... 999 µL/min
If the EP and the stop drift have been reached the titration will be stopped.
This parameter is only shown for
Stop criterion
=
drift
.
Delay time
0 ... [ 10 ] ... 999 s
(Titrando 835, 836, 841),
0 ... [ 10 ] ... 999 s, inf.
(Titrino 720, 736, 751, 758, 784, 795, 799)
If the EP has been reached, after the last dosing the delay time here de-
fined is awaited and then the titration is stopped. This parameter is only
shown for
Stop criterion
=
time
.
inf.
stands for infinite.
Stop time
1 ... 999999 s
(only Titrino 720, 736, 751, 758, 784, 795, 799)
The titration is stopped if the defined stop time has elapsed. This parameter
is only shown for
Stop criterion
=
time
and
Delay time
=
inf.
Endpoint 2
(only visible for
EP1 at pH
≠
off
)
[ on ], off
Switching endpoint 2 on/off. If this is deactivated all following parameters
are not visible.