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Metrohm tiamo 1.0 Manual User Manual

Page 397

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Commands

373

Control

(only visible for

Titration rate

=

user

)

Dynamics pH

0.001 ... [ 2.000 (slow) ] ... [ 2.000 (optimal) ] ... [ 0.500 (fast) ] ... 20.000, off

(Titrando),

0.01 ... [ 2.00 (slow) ] ... [ 2.00 (optimal) ] ... [ 0.50 (fast) ] ... 20.00, off

(Titrino)

Dynamics defines the measured value range before the given endpoint.
This parameter has an important influence on the titration rate and with it on
the accuracy. Within the control range the steps which are added are con-

trolled by the

Min. rate

. The nearer the endpoint the slower the dosing takes

place until the

Min. rate

has been reached. Outside the range the dosing

takes place with

Max. rate

) (see Control range).

Max. rate

0.01 ... [ 1.00 (slow) ] ... [ 10.00 (optimal) ] ... 166.00 mL/min, [ maximal (fast) ]

(Titrando)

0.01 ... [ 1.00 (slow) ] ... [ 10.00 (optimal) ] ... 150.00 mL/min, [ maximal (fast) ]

(Titrino)
Speed of addition outside the control range. The maximum dosing speed
depends on the cylinder volume of the exchange unit or dosing unit used.

Min. rate

0.01 ... [ 5.00 (slow)] ... [ 25.00 (optimal) ] ... [ 50.00 (fast) ] ... 9999.00 µL/min

Speed of addition at the start and finish of the titration. The slower the

minimum rate that is selected, the slower the titration and the higher the ac-
curacy.

Stop criterion

Stop criterion

[ drift ], time, off

The titration stops when the endpoint has been reached and the stop crite-

rion has been fulfilled. The titration can be stopped when a particular

drift

has been achieved or after a preset

time

. If no stop criterion has been se-

lected the titration will not be stopped.

Note

The Stop conditions will always stop the titration even if the stop criterion has not
been fulfilled or has been turned off.

Stop drift

1 ... [ 20 ] ... 999 µL/min

If the EP and the stop drift have been reached the titration will be stopped.
This parameter is only shown for

Stop criterion

=

drift

.

Delay time

0 ... [ 10 ] ... 999 s

(Titrando 835, 836, 841),

0 ... [ 10 ] ... 999 s, inf.

(Titrino 720, 736, 751, 758, 784, 795, 799)

If the EP has been reached, after the last dosing the delay time here de-
fined is awaited and then the titration is stopped. This parameter is only

shown for

Stop criterion

=

time

.

inf.

stands for infinite.

Stop time

1 ... 999999 s

(only Titrino 720, 736, 751, 758, 784, 795, 799)

The titration is stopped if the defined stop time has elapsed. This parameter
is only shown for

Stop criterion

=

time

and

Delay time

=

inf.

Endpoint 2

(only visible for

EP1 at pH

off

)

[ on ], off

Switching endpoint 2 on/off. If this is deactivated all following parameters
are not visible.