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Changing the izs permeation tube, Maintaining the so2 scrubber, Maintaining the so – Teledyne 6200E - Sulfides Analyzer User Manual

Page 194: Scrubber, Predicting when the so, Scrubber should be replaced

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Instrument Maintenance

Model 6200E Instruction Manual

194

M6200E Rev: A1

5. Re-install the PTFE O-ring with the notches facing up, the glass cover, then screw on the hold-

down ring and hand-tighten the assembly. Inspect the (visible) seal between the edge of the

glass window and the O-ring to assure proper gas tightness.

6. Re-start the analyzer.

9.3.2. Changing the IZS Permeation Tube

1. Turn off the analyzer, unplug the power cord and remove the cover.

2. Locate the IZS oven in the rear left of the analyzer.

3. Remove the top layer of insulation if necessary.

4. Unscrew the black aluminum cover of the IZS oven (3 screws) using a medium Phillips-head

screw driver. Leave the fittings and tubing connected to the cover.

5. Remove the old permeation tube if necessary and replace it with the new tube. Make sure that

the tube is placed into the larger of two holes and that the open permeation end of the tube
(plastic) is facing up.

6. Re-attach the cover with three screws and make sure that the sealing O-ring is properly in

place and that the three screws are tightened evenly.

7. Replace the analyzer cover, plug the power cord back in and turn on the analyzer.

8. Carry out an IZS span check to see if the new permeation device works properly. The

permeation rate may need several days to stabilize.

WARNING

Do not leave instrument turned off for more than 8 hours without

removing the permeation tube. Do not ship the instrument without

removing the permeation tube. The tube continues to emit gas, even at

room temperature and will contaminate the entire instrument.

9.3.3. Maintaining the SO

2

Scrubber

The SO

2

scrubber of your M6200E utilizes a consumable compound to absorb SO

2

form the sample

gas that must be replaced periodically in order for the analyzer to continue measuring H

2

S

accurately and reliability.

This material is capable of efficiently scrubbing SO

2

for up to 1000 ppm/hours. This means that if

the SO

2

content of the sample gas is typically around 100 ppb, the scrubber will function for

approximately 10 000 hours, a little over 13 months. If, however, the typical ambient SO

2

level

of the sample gas is 250 ppb, the scrubber would only last for approximately 4000 hours or about

5 ½ months.

9.3.3.1. Predicting When the SO

2

Scrubber Should Be Replaced.

To determine how long the SO

2

scrubber will operate efficiently: