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6 set titration – Metrohm 916 Ti-Touch User Manual

Page 420

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30.6 SET titration

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916 Ti-Touch

Problem

Cause

Remedy

A button in the
manual control is
disabled.

The required hardware is
either not connected or
incorrectly connected.

1. Switch off the 916 Ti-Touch.
2. Connect the hardware correctly.
3. Switch the 916 Ti-Touch back on.

The required hardware is
being used in the ongoing
determination.

Wait until the determination is finished.

30.6

SET titration

Problem

Cause

Remedy

The titration will not
be finished.

The minimum dosing rate
is too low.

Define Titration rate = user and increase the
minimum rate (Min. rate) (see Chapter
28.3.2, page 310)
.

The stop criterion is unsuit-
able.

Adjust the control parameters (see Chapter
28.3.2, page 310)
:

Increase the stop drift.

Select a short delay time.

The sample is over-
titrated.

The control parameters are
unsuitable.

Adjust the control parameters (see Chapter
28.3.2, page 310)
:

Select Titration rate = slow.

Define Titration rate = user and increase
the control range.

Define Titration rate = user and reduce
the maximum rate (Max. rate).

Define Titration rate = user and reduce
the minimum rate (Min. rate).

Stir faster.

Arrange the electrode and buret tip to an
optimum .

The electrode responds too
slowly.

Replace the electrode.

The titration time is
too long.

The control parameters are
unsuitable.

Adjust the control parameters (see Chapter
28.3.2, page 310)
:

Select Titration rate = optimal or fast.

Define Titration rate = user and reduce
the control range.

Define Titration rate = user and increase
the maximum rate (Max. rate).