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Metrohm 726 Titroprocessor User Manual

Page 138

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8.2 DET

726 Titroprocessor, Instructions for use

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Dos. rate

Dosing rate of initial dosing

0.01 mL/min…150 mL/min | max.

The maximum dosing rate will depend on the size of the

buret cylinder used.

Buret cylinder max. rate

1 mL

3 mL/min

2 mL

6 mL/min

5 mL

15 mL/min

10 mL

30 mL/min

20 mL

60 mL/min

50 mL

150 mL/min

A value up to 150 mL/min can be entered even for small

buret cylinders. When the method is executed, however,

the dosing rate will be automatically reduced to the largest

possible value. Select 'max' whenever possible, except with

viscous reagent solutions.

Meas.val.

Measured value for discontinuing initial dosing

with DET_PH:

pH -20 … 20 | off

with DET_U, DET_IPOL:

-2000 … 2000 mV | off

with DET_UPOL:

-200 … 200 µA | off

The threshold value of the measured signal, on attainment

of which initial dosing is discontinued. The controlled titra-

tion and data recording will then start after the pre-defined

pause (if programmed).

The direction and the progress of the change in measured

value have no incidence on the detection of this threshold

value. The measured value must be exceeded anyway.

Slope

Signal slope for discontinuing initial dosing

with DET_PH:

0.1 … 9.99 pH/mL | off

with DET_U, DET_IPOL:

0.5 … 999 mV/mL | off

with DET_UPOL:

0.1 … 99.9 µA/mL | off

The maximum value of the change in measured signal per

millilitre, on attainment of which initial dosing is discontin-

ued.

The controlled titration and data recording will then start

after the pre-defined pause (if programmed).

Pause

Pause before start of controlled titration

0 … 9999 s

A pause can be inserted before controlled titration starts. If

initial dosing is programmed, the pause will start on com-

pletion of this initial dosing.