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3 operating tutorial, 1 requirements, 3operating tutorial – Metrohm 732 IC Detector User Manual

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3.1 Requirements

732 IC Detector / 733 IC Separation Center

45

3

Operating tutorial

This section introduces you to the operation of the 732 IC Detector

and 733 IC Separation Center by means of a brief operating tutorial

which describes the basic operating steps needed for the recording

of an ion chromatogram and the development of a method.
The determination of the anionic content of a drinking water sample

with the PRP-X100 IC Anion Column using the single column tech-

nique is used an illustrative example. Please note that the steps and

parameter settings described apply only to this example. If you per-

form a different determination, use a different separating column or

other peripheral units, the procedures described in the tutorial must

be modified appropriately.
For further explanations of the operation, please refer to section 4,

which describes the functions of the individual keys and the pro-

gramming in detail.

3.1

Requirements

For the determination of anions in drinking water described in this tuto-

rial, the following instruments, accessories and solutions are required:

2.732.0X10 IC Detector

2.733.0XX0 IC Separation Center

without connection of the suppressor module

100

µµL Sample loop (6.2620.120 steel or 6.1825.220 PEEK)

already integrated in the 2.733.0010 and

2.733.0X20 IC Separation Center

2.709.0X10 IC Pump

In the operating tutorial, the pump is connected to the

732 IC Detector and remote controlled by this.

6.2125.060 Cable (connecting cable 732 – 709)

RS232 connecting cable for remote control of the

709 IC Pump by the 732 IC Detector.

6.2620.150 Pulsation dampener

Use of the pulsation dampener available as an option is

optional, but is advisable to protect the separating column.