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3 operating tutorial, 4 operation – Metrohm 732 IC Detector User Manual

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Table of contents

732 IC Detector / 733 IC Separation Center

II

2.8 Separating columns and suppressor module.................................... 32

2.8.1

General information on separating columns .............................. 32

2.8.2

Selection of the sample loop ...................................................... 32

2.8.3

General information on suppressor module............................... 33

2.8.4

One-channel system without suppressor module...................... 35

2.8.5

Two-channel system without suppressor module...................... 35

2.8.6

One-channel system with suppressor module........................... 37

2.8.7

Leak testing and conditioning..................................................... 40

2.9 Connection of external devices............................................................ 41

2.9.1

Connection of a recorder ............................................................ 41

2.9.2

Connection of «IC Metrodata for Win95».................................... 41

2.9.3

Connection of the 750 Autosampler ........................................... 41

2.9.4

Connection of the 766 IC Sample Processor ............................. 41

2.9.5

Connection of the 791 VA Detector ............................................ 41

2.9.6

Connection of a printer ............................................................... 42

2.9.7

Connection of a PC..................................................................... 44

2.9.8

Connection of devices to the remote interface........................... 44

3 Operating tutorial

........................................................................

45

3.1 Requirements .......................................................................................... 45
3.2 Preparations............................................................................................. 46
3.3 Putting into operation ............................................................................ 48
3.4 Calibration................................................................................................ 59
3.5 Sample determination ............................................................................ 62
3.6 Storing as a method ............................................................................... 64

4 Operation

...............................................................................................

67

4.1 Operating sequences ............................................................................. 67

4.1.1

General flow chart ....................................................................... 67

4.1.2

Flow chart for basic settings ....................................................... 68

4.1.3

Flow chart for putting into operation ........................................... 69

4.1.4

Flow chart for injection ................................................................ 70

4.2 Fundamentals of the operation ............................................................ 71

4.2.1

Display......................................................................................... 71

4.2.2

Overview of key functions ........................................................... 72

4.2.3

Instrument dialog ........................................................................ 77

4.2.4

Data entry.................................................................................... 79

4.2.5

Text entry..................................................................................... 80

4.3 Displays in the standby mode .............................................................. 81

4.3.1

Measured value and current time ............................................... 81

4.3.2

Status messages ........................................................................ 82

4.4 Basic settings.......................................................................................... 84

4.4.1

Setup ........................................................................................... 84

4.4.2

Configuration, key.................................................. 88

4.5 Measurement parameters...................................................................... 97

4.5.1

key ........................................................................... 97

4.5.2

key................................................................. 102