beautypg.com

6 triggering of functions, Fill> keys, Inject> keys – Metrohm 732 IC Detector User Manual

Page 110: Zero> key, Zero off> key, Mark> key, Pump r/s> key

background image

4.6 Triggering of functions

732 IC Detector / 733 IC Separation Center

103

4.6

Triggering of functions

4.6.1

keys

The two keys at the 733 IC Separation Center each have the

following function, which depends on the instrument version:

733.0010 (1 valve)

733.0X20 (2 valves)

733.0X30 (valve+ suppr.)

FILL

A

Switching of injection

valve A to "FILL"

position

Switching of injection

valve A to "FILL"

position

Switching of injection

valve A to "FILL"

position

STEP

FILL

B

No function

Switching of injection

valve B to "FILL"

position

Switching of suppres-

sor module to next

position ("STEP"

function)

If the injection valve is in the

"FILL" position, the green LED in

the key lights up. In this position

the injection valve is connected

as shown in the diagram oppo-

site:

The sample loop is filled by

siphoning in the sample so-

lution using the syringe.

The eluent flows directly to

the separating column.

The "FILL" function can be triggered at any time with the key –

also in the edit mode or when a program is running. If this is not re-

quired, the key can be locked. For this, the parameter

"

>CONFIG/733

IC

Sep.Cent./control

"

must be set to

"

732 only

"

under the

key (see section 4.4.2). Switching of the injection valve is then possible

only using the 732 IC Detector via a programmed "FILL" command or

with

"

>CONFIG/733

IC

Sep.Cent./trigger = fill

"

.

With the 733.0030 IC Separation Center, switching of the suppressor

module to the next position can be triggered automatically by the

switching of injection valve A to the "FILL" position. For this, the pa-

rameter

"

>CONFIG/733/suppressor/auto step

"

must be set to

"

fill

"

under the key (see section 4.4.2).

1

2

4

5

3

6

Syringe

Column

Eluent

Sample

Loop