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Metrohm 732 IC Detector User Manual

Page 150

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5.2 Maintenance and servicing

732 IC Detector / 733 IC Separation Center

143

7 Insert connection piece

Insert connection piece 98

98 in suppressor holder 100

100 in such

a way that connection "1" is at the top, and that the three lugs

on the connection piece fit in the corresponding openings of

the holder.

Screw nut 97

97 onto the thread of suppressor holder 100

100

manually (do not use tools).

8 Connect and condition the suppressor

Reconnect the suppressor to the IC system.

Before switching the suppressor to the next position for the

first time, rinse all 3 suppressor units with solution for 5 min.

5.2.8

Replacing the suppressor

The suppressor in the suppressor block may have to be replaced in the

following cases:

Irremediable loss of suppressor capacity (reduced

phosphate sensitivity and/or strong rise in baseline)

Irremediable blockage of the suppressor (the suppres-

sor can no longer deliver solutions)

Both the 6.2832.000 Suppressor rotor and the 6.2832.010 Connection

piece with the input and output leads can be replaced. To replace

these components proceed as follows (see Fig. 24):

1 Disconnect suppressor from IC system

Disconnect all input and output leads of the suppressor from

IC system and the pump of the 752 Pump Unit.

2 Dismantle suppressor

Unscrew nut 97

97 from suppressor holder 100

100.

Pull out connection piece 98

98 and suppressor rotor 99

99 from

suppressor holder 100

100 (the connection piece and the rotor

normally stick together).

Loosen connection piece 98

98 from suppressor rotor 99

99.

3 Clean suppressor rotor

Clean the sealing surface of new suppressor rotor 99

99

(6.2832.000) using a lint-free cloth and ethanol.

4 Insert suppressor rotor

Insert new suppressor rotor 99

99 in suppressor holder 100

100 in

such a way that the tubing connections at the rear of the rotor

fit in the corresponding openings inside the rotor and that one

of the three holes in the rotor can be seen from below in one

of the openings of the holder.