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5 determinations with voltammetric trace analysis, Load a determination – Metrohm 797 VA Computrace User Manual

Page 223

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8.5 Determinations with voltammetric trace analysis

797 VA Computrace – Software

211

6. If Dosing Devices should be used for addition or predose, click

and set the parameters to the desired values (see

Dosing Devices, section 5.2).

7. If necessary, click

and limit the

Highest current

range

or

Lowest current range

in the

POTENTIOSTAT

window

(see Potentiostat, section 3.3).

8. Click

and set the parameters on the tabs

Deter-

mination

,

Voltammetric

,

Substances

,

Calculations

,

Documenta-

tion

und

Export

(see section 5.2) in the

EDIT WORKING

METHOD PARAMETERS

window.

9. Close

the

EDIT WORKING METHOD PARAMETERS

window by

clicking

.

Modify methods for automatic background compensation

1. Click on

or

MAIN WINDOW

/ Mode / Determination

.

2. Click on

or

MAIN WINDOW

/ Window / Working method

specification

to open the

WORKING METHOD SPECIFICATIONS

window.

3. Click on

or

MAIN WINDOW

/ File / Load method

.

4. Select the desired method file

*.mth

in the

OPEN

window and

click

. The method is loaded into the

WORKING METHOD

SPECIFICATIONS

window.

5. Click the

button in the

WORKING METHOD SPE-

CIFICATIONS

window

and select the

Determination

tab.

6. Enable

the

Measure blank

option, enter the number of measu-

rements

No. of blanks

and the

Blank purge time

.

7. Close

the

EDIT WORKING METHOD PARAMETERS

window by

clicking

.

If you start a determination with this modified method, you are first
asked to place the specified number of blank solutions into the
measuring vessel. The resulting blank curve is then automatically
subtracted from all subsequent measured curves.

8.5

Determinations with voltammetric trace analysis

Load a determination

1. Click on

or

MAIN WINDOW

/ Mode / Determination

.

2. Click on

or

MAIN WINDOW

/ File / Load determination

.