5 determinations with voltammetric trace analysis, Load a determination – Metrohm 797 VA Computrace User Manual
Page 223

8.5 Determinations with voltammetric trace analysis
797 VA Computrace – Software
211
6. If Dosing Devices should be used for addition or predose, click
and set the parameters to the desired values (see
Dosing Devices, section 5.2).
7. If necessary, click
and limit the
Highest current
range
or
Lowest current range
in the
POTENTIOSTAT
window
(see Potentiostat, section 3.3).
8. Click
and set the parameters on the tabs
Deter-
mination
,
Voltammetric
,
Substances
,
Calculations
,
Documenta-
tion
und
Export
(see section 5.2) in the
EDIT WORKING
METHOD PARAMETERS
window.
9. Close
the
EDIT WORKING METHOD PARAMETERS
window by
clicking
.
Modify methods for automatic background compensation
1. Click on
or
MAIN WINDOW
/ Mode / Determination
.
2. Click on
or
MAIN WINDOW
/ Window / Working method
specification
to open the
WORKING METHOD SPECIFICATIONS
window.
3. Click on
or
MAIN WINDOW
/ File / Load method
.
4. Select the desired method file
*.mth
in the
OPEN
window and
click
. The method is loaded into the
WORKING METHOD
SPECIFICATIONS
window.
5. Click the
button in the
WORKING METHOD SPE-
CIFICATIONS
window
and select the
Determination
tab.
6. Enable
the
Measure blank
option, enter the number of measu-
rements
No. of blanks
and the
Blank purge time
.
7. Close
the
EDIT WORKING METHOD PARAMETERS
window by
clicking
.
If you start a determination with this modified method, you are first
asked to place the specified number of blank solutions into the
measuring vessel. The resulting blank curve is then automatically
subtracted from all subsequent measured curves.
8.5
Determinations with voltammetric trace analysis
Load a determination
1. Click on
or
MAIN WINDOW
/ Mode / Determination
.
2. Click on
or
MAIN WINDOW
/ File / Load determination
.