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Metrohm 797 VA Computrace User Manual

Page 104

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5 Determination mode

797 VA Computrace – Software

92

Cell volume (mL) [ > 0 mL ; 10 mL ]

Total volume of solution (sample + auxiliary solu-
tion, e.g. buffer (added manually or pre-dosed
with a Dosing Device)) in the measuring vessel at
the start of the determination. The sample con-
centrations

Conc.

calculated refer to this cell vo-

lume.

Note: The sample and solution parameters (

Sample identifier

,

Sample amount

,

Sample unit

,

Cell volume

) are different with the

CVS or CPVS mode.

Measure blank [ on, off ; off ]

Measure a blank solution before sample determi-
nation. The blank curve is then automatically sub-
tracted from all subsequent measured curves. This
background compensation

is mainly used to re-

duce interference due to the supporting electro-
lyte. Such interference includes both the presence
of the analyte (blank value) and that of foreign
substances electroactive in the same range.

No. of blanks [ 1...5 ; 1 ]

Number of measurements to determine the blank
curve. If the blank solution is measured several
times, a mean blank curve is determined from the
different measurements.

Blank purge time [ 0...80600 s ; 300 s ]

Time of inert gas purging before measurement of
the blank solution.

Addition purge time [ 0...80600 s ; 10 s ]

Time of inert gas purging for all measurements af-
ter determination of the sample (standard addi-
tion) or of the first calibration solution if

Batch

is

selected for

Technique

(for the first measurement,

the

Initial purge time

is used).

Note: The blank measurements parameters (

Measure blank

,

No. of

blanks

,

Blank purge time

,

Addition purge time

) are different with

the CVS or CPVS mode.

Cell purge time [ 0...80600 s ; 10 s ]

Time of inert gas purging after solution exchange
if

Batch with solution exchange

is selected for

Technique

.

No. of additions [ 0...28 ; 2 ]

Number of additions of standard addition solu-
tions

resp.

calibration solutions if

Batch

is selected

for

Technique

.