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Teledyne 9110EH - Nitrogen Oxides Analyzer User Manual

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Model 9110EH Instruction Manual M9110EH Documentation

6.10.2.3. Editing iDAS Data Channels ........................................................................... 95

6.10.2.4. Trigger Events ............................................................................................. 97

6.10.2.5. Editing iDAS Parameters ............................................................................... 98

6.10.2.6. Sample Period and Report Period ................................................................. 100

6.10.2.7. Number of Records .................................................................................... 101

6.10.2.8. RS-232 Report Function .............................................................................. 102

6.10.2.9. Compact Report......................................................................................... 103

6.10.2.10. Starting Date........................................................................................... 103

6.10.2.11. Disabling/Enabling Data Channels............................................................... 103

6.10.2.12. HOLDOFF Feature..................................................................................... 104

6.10.3. Remote iDAS Configuration................................................................................ 105

6.11. Remote Operation of the Analyzer............................................................................. 106

6.11.1. Basic Operation................................................................................................ 106

6.11.1.1. Terminal Operating Modes........................................................................... 106

6.11.1.2. Help Commands in Terminal Mode................................................................ 107

6.11.1.3. Command Syntax ...................................................................................... 107

6.11.1.4. Data Types ............................................................................................... 108

6.11.2. Status Reporting .............................................................................................. 108

6.11.3. Remote Access by Modem ................................................................................. 109

6.11.4. COM Port Password Security .............................................................................. 110

6.11.5. APICOM Remote Control Program ....................................................................... 111

6.11.6. Additional Communications Documentation .......................................................... 112

7. CALIBRATION PROCEDURES ..........................................................................................113

7.1. Calibration Preparations ............................................................................................ 113

7.1.1. Required Equipment, Supplies, and Expendables .................................................... 113

7.1.2. Zero Air............................................................................................................ 113

7.1.3. Span Gas Standards ........................................................................................... 113

7.1.4. NO

2

Permeation Tubes ........................................................................................ 114

7.1.5. Calibration Gas Traceability ................................................................................. 114

7.1.6. Data Recording Devices ...................................................................................... 114

7.1.7. NO

2

Conversion Efficiency ................................................................................... 114

7.2. Manual Calibration.................................................................................................... 116

7.2.1. Connect Zero Air and Span Gases to the Analyzer................................................... 117

7.2.2. Set Expected NO and NO

X

Span Gas Concentrations................................................ 117

7.2.3. Perform Zero/Span Calibration:............................................................................ 118

7.3. Calibration Checks.................................................................................................... 119

7.4. Calibration with Zero/Span Valves .............................................................................. 119

7.5. Calibration with IZS Option ........................................................................................ 120

7.6. Calibration Checks with IZS or Zero/Span Valves .......................................................... 123

7.7. Calibration With Independent or AUTO Ranges.............................................................. 124

7.7.1. Calibration in AUTO Range Mode .......................................................................... 124

7.7.2. Independent Range Mode.................................................................................... 125

7.7.3. Calibration With Remote Contact Closures ............................................................. 125

7.8. Automatic Calibration (AutoCal).................................................................................. 126

7.9. Calibration Quality Analysis........................................................................................ 128

8. EPA PROTOCOL CALIBRATION .......................................................................................131

8.1. Calibration of Equipment ........................................................................................... 131

8.2. Gas Phase Titration (GPT).......................................................................................... 133

8.2.1. GPT Principle of Operation ................................................................................... 133

8.2.2. GPT Calibrator Check Procedure ........................................................................... 133

8.2.3. Example GPT Calculation..................................................................................... 134

8.3. Multipoint Calibration Procedure ................................................................................. 136

8.3.1. Zero Calibration ................................................................................................. 137

8.3.2. Span Calibration ................................................................................................ 137

8.3.3. GPT NO

2

Calibration ........................................................................................... 138

8.4. Calibration Frequency ............................................................................................... 139

8.5. Other Quality Assurance Procedures............................................................................ 139

8.6. Summary of Quality Assurance Checks ........................................................................ 140

8.7. Short Calibration Checks ........................................................................................... 141

8.7.1. Zero/Span Check Procedures ............................................................................... 141

M9110EH

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