Teledyne 9110E - Nitrogen Oxides Analyzer - Manual (Page 5)

Model 9110E Instruction Manual M9110E Documentation
M9110E Rev B v
6.10.2.3. Editing iDAS Data Channels ............................................................................ 95
6.10.2.4. Trigger Events............................................................................................... 97
6.10.2.5. Editing iDAS Parameters................................................................................. 98
6.10.2.6. Sample Period and Report Period................................................................... 100
6.10.2.7. Number of Records ...................................................................................... 101
6.10.2.8. RS-232 Report Function ............................................................................... 102
6.10.2.9. Compact Report .......................................................................................... 103
6.10.2.10. Starting Date ............................................................................................ 103
6.10.2.11. Disabling/Enabling Data Channels ................................................................ 103
6.10.2.12. HOLDOFF Feature ...................................................................................... 104
6.10.3. Remote iDAS Configuration ................................................................................. 105
6.11. Remote Operation of the Analyzer .............................................................................. 106
6.11.1. Basic Operation ................................................................................................. 106
6.11.1.1. Terminal Operating Modes ............................................................................ 106
6.11.1.2. Help Commands in Terminal Mode ................................................................. 107
6.11.1.3. Command Syntax ........................................................................................ 107
6.11.1.4. Data Types ................................................................................................. 108
6.11.2. Status Reporting ................................................................................................ 108
6.11.3. Remote Access by Modem ................................................................................... 109
6.11.4. COM Port Password Security................................................................................ 110
6.11.5. APICOM Remote Control Program......................................................................... 111
6.11.6. Additional Communications Documentation ........................................................... 112
7. CALIBRATION PROCEDURES ..........................................................................................113
7.1. Calibration Preparations .............................................................................................. 113
7.1.1. Required Equipment, Supplies, and Expendables ..................................................... 113
7.1.2. Zero Air .............................................................................................................. 113
7.1.3. Span Gas Standards............................................................................................. 113
7.1.4. NO
2
Permeation Tubes.......................................................................................... 114
7.1.5. Calibration Gas Traceability................................................................................... 114
7.1.6. Data Recording Devices ........................................................................................ 114
7.1.7. NO
2
Conversion Efficiency ..................................................................................... 114
7.2. Manual Calibration...................................................................................................... 116
7.2.1. Connect Zero Air and Span Gases to the Analyzer.................................................... 117
7.2.2. Set Expected NO and NO
X
Span Gas Concentrations................................................. 117
7.2.3. Perform Zero/Span Calibration: ............................................................................. 118
7.3. Calibration Checks...................................................................................................... 119
7.4. Calibration with Zero/Span Valves ................................................................................ 119
7.5. Calibration with IZS Option.......................................................................................... 120
7.6. Calibration Checks with IZS or Zero/Span Valves ........................................................... 123
7.7. Calibration With Independent or AUTO Ranges............................................................... 124
7.7.1. Calibration in AUTO Range Mode............................................................................ 124
7.7.2. Independent Range Mode ..................................................................................... 125
7.7.3. Calibration With Remote Contact Closures............................................................... 125
7.8. Automatic Calibration (AutoCal) ................................................................................... 126
7.9. Calibration Quality Analysis ......................................................................................... 128
8. EPA PROTOCOL CALIBRATION .......................................................................................131
8.1. Calibration of Equipment ............................................................................................. 131
8.2. Gas Phase Titration (GPT) ........................................................................................... 133
8.2.1. GPT Principle of Operation..................................................................................... 133
8.2.2. GPT Calibrator Check Procedure............................................................................. 133
8.2.3. Example GPT Calculation ...................................................................................... 134
8.3. Multipoint Calibration Procedure ................................................................................... 136
8.3.1. Zero Calibration................................................................................................... 137
8.3.2. Span Calibration .................................................................................................. 137
8.3.3. GPT NO
2
Calibration ............................................................................................. 138
8.4. Calibration Frequency ................................................................................................. 139
8.5. Other Quality Assurance Procedures ............................................................................. 139
8.6. Summary of Quality Assurance Checks ......................................................................... 140
8.7. Short Calibration Checks ............................................................................................. 141
8.7.1. Zero/Span Check Procedures................................................................................. 141