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Sensor module, reaction cell & pmt – Teledyne 9110E - Nitrogen Oxides Analyzer User Manual

Page 192

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Theory of Operation

Model 9110E Instruction Manual

178

M9110E Rev B

10.3.1.2. Flash Chip

The flash chip is another, smaller EEPROM with about 64 kb of space, internally labeled as

DOS drive B:\. The M9110E CPU board can accommodate up to two EEPROM flash chips.
The M9110E standard configuration is one chip with 64 kb of storage capacity, which is

used to store the analyzer configuration as created during final checkout at the factory.

Separating these data onto a less frequently accessed chip significantly decreases the

chance of data corruption through drive failure.

In the unlikely event that the flash chip should fail, the analyzer will continue to operate
with just the DOC. However, all configuration information will be lost, requiring the unit to

be recalibrated.

10.3.2. Sensor Module, Reaction Cell & PMT

Electronically, the M9110E sensor assembly (Figure 10-14) consists of several

subassemblies with different tasks: to detect the intensity of the light from the

chemiluminescence reaction between NO and O

3

in the reaction cell, to produce a current

signal proportional to the intensity of the chemiluminescence, to control the temperature of
the PMT to ensure the accuracy and stability of the measurements and to drive the high

voltage power supply that is needed for the PMT. The individual functions are described
individually below, Section 11.6.6 shows the sensor assembly and its components.

10.3.2.1. Reaction Cell Heating Circuit

The stability of the chemiluminescence reaction between NO and O

3

can be affected by

changes in the temperature and pressure of the O

3

and sample gases in the reaction cell. In

order to reduce temperature effects, the reaction cell is maintained at a constant 50° C, just
above the high end of the instrument’s operation temperature range.

Two AC heaters, one embedded into the bottom of the reaction cell, the other embedded
directly above the chamber’s exhaust fitting, provide the heat source. These heaters

operate off of the instrument’s main AC power and are controlled by the CPU through a
power relay on the relay board (Section 10.3.4). A thermistor, also embedded in the bottom

of the reaction cell, reports the cell’s temperature to the CPU through the thermistor

interface circuitry of the motherboard (Section 10.3.5).

10.3.2.2. Photo Multiplier Tube (PMT)

The M9110E uses a photo multiplier tube (PMT) to detect the chemiluminescence created by

the reaction of NO with O

3

in the reaction cell.

A typical PMT is a vacuum tube containing a variety of specially designed electrodes

(Figure 10-14). Photons from the reaction are filtered by an optical high-pass filter, enter
the PMT and strike a negatively charged photo cathode causing it to emit electrons. A high

voltage potential across these focusing electrodes directs the electrons toward an array of
high voltage dynodes. The dynodes in this electron multiplier array are designed so that

each stage multiplies the number of emitted electrons by emitting multiple, new electrons.
The greatly increased number of electrons emitted from one end of electron multiplier are

collected by a positively charged anode at the other end, which creates a useable current

signal. This current signal is amplified by the preamplifier board and then reported to the

motherboard.