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Zero calibration, Span calibration – Teledyne 9110E - Nitrogen Oxides Analyzer User Manual

Page 151

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Model 9110E Instruction Manual

EPA Protocol Calibration

M9110E Rev B

137

Figure 8-1: GPT Calibration System

Converter efficiency should be set prior to calibration since its value is used in the

computation of the NO

X

and NO

2

concentration outputs.

The analyzer should be calibrated on the same range used for monitoring.

If auto ranging or independent range options are selected the highest of the ranges will

result in the most accurate calibration, and should be used.

Make sure the GPT calibration system can supply the range of concentrations at a sufficient

flow over the whole range of concentrations that will be encountered during calibration.

8.3.1. Zero Calibration

The zero point calibration procedure is identical to that described in Sections 7.2, 7.4 or 7.5

of this manual.

8.3.2. Span Calibration

Adjust the NO concentration to approximately 80% of the URL of the NO channel. The

expected NO and NO

X

span concentrations can be determined by measuring the cylinder

and diluent flows and computing the resulting concentrations. If there is any NO

2

impurity

in the NO standard gas it should be taken into account when the NO

X

concentration is

entered during the NO/NO

X

channel calibration. This is done by ADDING the impurity

concentration to the NO concentration to get the NO

X

concentration for calibration.

Calculate the exact NO and NO

X

concentrations as follows: