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Sample gas flow – Teledyne 9110E - Nitrogen Oxides Analyzer User Manual

Page 180

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Theory of Operation

Model 9110E Instruction Manual

166

M9110E Rev B

Figure 10-5: External Pump Pack

Finally, the M9110E requires a steady, high underpressure, which cannot be achieved

reliably over extended periods of time with small vacuum pumps. The external pump used

for the M9110E has a very long lifetime and duty cycle and provides a very good vacuum

for its entire lifetime. However, the pump is too large to fit into the chassis of the analyzer.

10.2.2. Sample Gas Flow

The sample gas is the most critical flow path in the analyzer, as the medium has to be

routed through a variety of valves and tubes for the measurement of zero offset and

concentrations of both NO and NO

X

(and possibly the drying of the gas if the optional

sample dryer is installed). At any point before and in the reaction cell, the integrity of the

sample gas cannot be compromised.

Sample gas flow in the M9110E analyzer is not a directly measured value, but is rather

calculated from the sample pressure using the flow principle across a critical orifice. In

general, the differential pressure ratio between sample pressure and reaction cell pressure
needs to exceed 2:1 to allow critical flow. The actual flow rate is then only dependent on

the size of the orifice and the upstream pressure. Refer to Section 10.2.9 for a detailed

description of critical flow.

The M9110E uses a 0.010” (10 mil) diameter orifice to achieve a flow rate of about

450-500 cm³/min. With nominal pressures of 28 and 4 in-Hg-A for the sample and reaction

cell pressures, respectively. The necessary ratio of sample to reaction cell pressure of 2:1 is

largely exceeded and accommodates a wide range of possible variability in atmospheric
pressure and pump degradation. Once the pump degrades and vacuum pressure exceeds

14 in-Hg-A, the ratio between sample and vacuum pressures is less than 2:1 and, hence, a
critical flow rate can no longer be calculated. At this point, the instrument will display an

invalid sample flow rate measurement (XXXX).