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Min 2 f f v t, Ч + ч – Teledyne 9110E - Nitrogen Oxides Analyzer User Manual

Page 148

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EPA Protocol Calibration

Model 9110E Instruction Manual

134

M9110E Rev B

If more than one analyzer is to be calibrated at the same time, multiply F

T

by the number of

analyzers.

Calculate the NO concentration [NO]

OUT

needed to approximate 90% of the URL of the NO

2

analyzer to be calibrated, using Equation 8-2:

[NO]

OUT

= URL of analyzer (ppm) x 90/100

Eq 8-2

Calculate the NO flow (F

NO

) required to generate the NO concentration [NO]

OUT

, using

Equation 8-3:

]

[NO

F

x

]

[NO

=

F

STD

T

OUT

NO

Eq 8-3

Calculate the required flow through the ozone generator (F

O

), using Equation 8-4:

F

-

min

-

ppm

2.75

V

X

F

X

]

[NO

=

F

NO

RC

NO

STD

o

Eq 8-4

Verify that the residence time (t

R

) in the reaction cell is <2 min, using Equation 8-5:

min

2

F

F

V

t

NO

O

RC

R

+

=

Eq 8-5

Verify that the dynamic parameter specification (P

R

) of the calibrator's reaction cell is

>2.75 ppm-min using Equation 8-6:

[ ]

75

.

2

F

F

V

F

F

F

NO

P

NO

O

RC

NO

O

NO

STD

R

+

Ч

+

Ч

=

Eq 8-6

NOTE

If t

r

is >2 minutes or if P

R

is <2.75 ppm min, changes in flow conditions

(F

T

, F

O

, F

NO

) or in the reaction cell volume (V

RC

), or both will

have to be made, and t

r

and P

R

will have to be recalculated.

After equations 8-5 and 8-6 are satisfied, calculate the diluent air flow (F

D

) using

Equation 8-7:

NO

O

T

D

F

F

F

F

=

Eq 8-7

8.2.3. Example GPT Calculation

Following is an example calculation that can be used to determine whether an existing GPT
calibrator will meet the required conditions for a specific calibration. For this example, it is