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Calibration problems, Miss-calibrated, Non-repeatable zero and span – Teledyne GFC-7000E - Trace CO2 Analyzer User Manual

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Model GFC7000E Instruction Manual

TROUBLESHOOTING & REPAIR PROCEDURES

04584 Rev A1

195

ambient air, these natural, diurnal fluctuations might be detected by the instrument and cause its
in its calculation of the CO

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concentration of the sample gas to drift.

Another possible symptom of poor or stopped purge gas flow would be the inability to measure
zero concentrations accurately at the end of a work day on a system that was calibrated at the
beginning of a workday. Again this could be due to local fluctuations in ambient CO

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concentration between the time of the day when the calibration was performed and other times
during the day.

11.2. Calibration Problems

11.2.1. Miss-Calibrated

There are several symptoms that can be caused by the analyzer being miss-calibrated. This
condition is indicated by out of range Slopes and Offsets as displayed through the test functions
and is frequently caused by the following:

1. BAD SPAN GAS. This can cause a large error in the slope and a small error in the offset.

Delivered from the factory, the MGFC7000E’s slope is within ±15% of nominal. Bad span gas

will cause the analyzer to be calibrated to the wrong value. If in doubt have the span gas
checked by and independent lab.

2. CONTAMINATED ZERO GAS. Excess H

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O can cause a positive or negative offset and will

indirectly affect the slope.

3. Dilution calibrator not set up correctly or is malfunctioning. This will also cause the slope, but

not the zero to be incorrect. Again the analyzer is being calibrated to the wrong value.

4. Too many analyzers on the manifold. This can cause either a slope or offset error because

ambient gas with its pollutants will dilute the zero or span gas.

11.2.2. Non-Repeatable Zero and Span

As stated earlier, leaks both in the MGFC7000E and in the external system are a common source
of unstable and non-repeatable readings.

1. Check for leaks in the pneumatic systems as described in Section 9.3.3. Don’t forget to

consider pneumatic components in the gas delivery system outside the MGFC7000E. Such as:

• A change in zero air source such as ambient air leaking into zero air line, or;

• A change in the span gas concentration due to zero air or ambient air leaking into the

span gas line.

2. Once the instrument passes a leak check, do a flow check (see Section 9.3.4) to make sure

adequate sample is being delivered to the sensor assembly.

3. A failing IR photo-detector may be at fault. Check the CO2 MEAS and CO2 REF test

functions via the front panel display to make sure the signal levels are in the normal range

(See Appendix A) and are quiet.