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6 appendix – Metrohm 792 Basic IC User Manual

Page 195

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6 Appendix

792 Basic IC

186

Separating column 66

66

66

66

Changing ........................................144

Characteristic data..........................139

Connection at detector

block 38

38

38

38 ............................................33

Connection to suppressor

module 39

39

39

39.........................................39

Dead volume...................................140

Figure ...........................................33,37

Fixing............................................33,34

General information ..........................32

Information ........................................83

Installation with suppressor ..............34

Installation without suppressor.........32

Internal diameter ...............................83

Length ..........................................83,95

Ordering designations ....................169

Packing material ...............................83

Particle size .......................................83

Practical notes ................................139

Protection........................................139

Regeneration...................................140

Report .............................................107

Rinsing .........................................33,34

Separation efficiency ......................139

Serial number....................................83

Storage............................................140

Test results......................................112

Void volume ......................................83

Separation efficiency ..........................139

Separator

.............................................113

Serial number 17

17

17

17

Figure .................................................. 5

Service..........................................143,158
Servicing .............................................143

Set all

............................................123,124

Set peak end

..........................................93

Set peak start

.........................................93

Setting up the instrument......................13

Setup

................................................71,91

Show all

.................................................87

...........................................124

Show baseline and peaks

....................124

Shutdown ............................................144

SHUTDOWN

...........................................78

Shutdown hardware

...............................69

Sleeve 63

63

63

63

Figure ................................................31

Installation .........................................30

Sleeve 97

97

97

97

Figure ..............................................149

Slope

................................................90,91

Snap-action lever 43

43

43

43

Figure ........................................7,36,38

Install tubing cartridge ......................35

Raise tubing cartridge .............141,155

Software installation..............................19
Software settings ..................................64
SOP .....................................................158
Special tool 93

93

93

93

Figure ..............................................147

Ordering designation......................165

Remove piston seal 89

89

89

89...................146

Special tool 94

94

94

94

Figure ..............................................147

Install piston seal 89

89

89

89 .......................148

Ordering designation......................165

Spilled chemicals................................143

Split peaks

...........................................128

Splitting ........................................140,157

Spring 84

84

84

84

Figure.............................................. 147

Ordering designations.................... 168

Spring retainer 83

83

83

83

Figure.............................................. 147

Standard chromatogram .................... 139

Standard component

.................... 104,112

Standard equipment........................... 164
Standard operating procedures......... 158

Start determination

................................ 69

Start time for event................................ 93
Starter Kit (6.5325.000)

Ordering designation...................... 168

Starting

.................................................. 78

Startup hardware

................................... 69

Static charges....................................... 10

Statistical weight

................................. 104

Status bar....................................... 60,118
Status messages .................................. 78
Steel meshes 58

58

58

58

Figure................................................ 29

Installation......................................... 28

Ordering designation...................... 174

................................................... 74

Stop determination

................................ 70

Stopper 73

73

73

73

Figure................................................ 36

Install pump tubing......................... 155

Install pump tubings ......................... 35

Strap (Y.107.0150)................................ 40

Subtract

............................................... 131

Subtraction of a chromatogram ......... 131
Sunlight ................................................. 13
Supply bottle......................................... 38
Suppression.......................................... 35

Suppressor

.................................. 74,75,76

Suppressor holder 105

105

105

105

Figure.............................................. 153

Mounting......................................... 154

Suppressor inlet capillary 75

75

75

75

Figure........................................... 38,40

Installation......................................... 39

Suppressor inlet capillary 77

77

77

77

Figure...................................... 36,38,40

Installation......................................... 40

Suppressor inlet capillary 78

78

78

78

Figure...................................... 36,38,40

Installation......................................... 39

Suppressor module 39

39

39

39

Autostep............................................ 76

Break time......................................... 77

Capacity.......................................... 142

Cleaning.......................................... 151

Connection ....................................... 39

Figure............................................. 7,38

General information ................... 35,142

Notes............................................... 142

Program instruction .......................... 75

Protection........................................ 142

Regeneration .................................. 150

Replacement................................... 153

Switching to next position................. 74

Technical data ................................ 161

Suppressor outlet capillary 76

76

76

76

Figure........................................... 38,40

Installation......................................... 39

Suppressor outlet capillary 79

79

79

79

Figure........................................... 38,40

Fixing................................................. 40

Installation......................................... 40

Suppressor outlet capillary 80

80

80

80

Figure........................................... 38,40

Fixing ................................................ 40

Installation......................................... 39

Suppressor rotor 104

104

104

104

Cleaning ......................................... 154

Figure.............................................. 153

Inserting .......................................... 154

Ordering designation ..................... 175

Replacement .................................. 153

Syringe (6.2816.020)

Aspirate sample................................ 54

Connection of syringe ...................... 14

Deaerate pump ................................ 25

Ordering designation ..................... 165

Syringe tubing 25

25

25

25

Figure.................................................. 7

Installation......................................... 14

System

Change ............................................. 68

Close................................................. 68

Conditioning ................................ 42,43

Definition...................................... 58,68

File handling ..................................... 68

File type ............................................ 61

Open................................................. 68

Print system parameters .................. 70

Save.................................................. 68

System functions.............................. 69

System settings ........................... 72,73

System startup values ...................... 74

System state window........................ 78

System window ................................ 68

SYSTEM

................................................ 59

System / Change

................................... 68

System / Close

...................................... 68

System / Save

........................................ 68

System startup values

...................... 69,74

System state

......................................... 78

SYSTEM STATE

............................. 59,156

T

Tab size

............................................... 113

Tabulated calibration..................... 94,103
Technical data .................................... 159

Temp.

.................................................... 84

Temperature ......................................... 84
Temperature dependence.................. 159
Temperature deviation ....................... 159
Temperature stability .......................... 159

Template

............................................. 113

Test chromatogram.............................. 32

Theoretical plates

........................... 88,115

Thermostatting.................................... 159

this color is default

............................. 125

This run

............................................... 100

Threshold for peak recognition ............ 91

Tic marks

............................................ 123

Time .................................. 70,81,82,93,97

Time axis

............................................. 122

Time program

Enable............................................... 75

Entry.................................................. 74

Report ............................................... 70

Verify ................................................. 75

Title bar ............................................... 118

................................... 120,132

Tool bar................................................. 60