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4 connection of the drain tube for bottle rack, 5 connection of peek capillaries – Metrohm 761 Compact IC User Manual

Page 27

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2.3 Attaching the accessories

761 Compact IC

17

2.3.4

Connection of the drain tube for bottle rack

The 761 Compact IC has a connection at the rear to which a drain tube

for discharged liquids in the bottle rack can be attached. Proceed as

follows:

1 Connect drain tube

Mount 6.1816.020 Silicone tubing on connection nipple 14

(see Fig. 2).

2 Lead drain tube to collecting vessel

Lead the other end of the drain tube to a suitable collecting

vessel and fix in place.

2.3.5

Connection of PEEK capillaries

For the connections between high-pressure pump and detector block

6.1831.010 PEEK capillaries (i.d. = 0.25 mm, e.d. =

1

/

16

"

) are used

which are connected using either 6.2744.010 PEEK compression fit-

tings (long) or 6.2744.070 PEEK compression fittings (short).

These PEEK connectors can also be used to connect 6.1822.010 PTFE

microcapillaries (i.d. = 0.3 mm). Proceed as follows:

Capillaries fitted with new connectors must have a perfectly flat cut

surface. To cut PEEK or PTFE capillaries it is best to use the

6.2621.080 Capillary tubing cutter.

1 Mount compression fitting

Slide a compression fitting 54 (6.2744.010) or a compression

fitting 55 (6.2744.070) over the end of the capillary 56 to be

fastened as shown in Fig. 7.

2 Insert capillary in connection

Push capillary end in the corresponding connection as far as it

will go (to avoid dead volume).

3 Tighten compression fitting

Tighten compression fitting 54 or 55 by hand (never use tools).

54 Compression fitting (6.2744.010)

55 Compression fitting (6.2744.070)

56 Capillary

6.1831.010 PEEK capillary or

6.1822.010 PTFE microcapillary

54

56

55

Fig. 7:

Connectors for capillaries