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3 injection valve, 4 high-pressure pump – Metrohm 761 Compact IC User Manual

Page 200

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6 Appendix

761 Compact IC

190

6.1.3 Injection valve

Actuator switching duration

100

150 ms

Pressure resistance

25 MPa (250 bar)

6.1.4 High-pressure pump

Type

Serial dual piston pump with two valves

Pump capacity

Flow range

0.20...2.5 mL/min

Maximum error

<

±

2 % of set value

Flow constancy

< 0.5 % of set value

Reproducibility of eluent

flow

typ. better than

±

0.1 %

Pressure measurement

Pressure range

0...25.0 MPa (0...250 bar)

Residual pulsation

< 1 % (at 1 mL/min water and 10 MPa pressure,

without pulsation dampener)

Measurement principle

Piezoresistive measurement

Response time: 3 ms

Measurement volume: ca. 50

µ

L

Maximum error

±

3 % of set value

Resolution

0.1 MPa (conductivity measurements)

0.01 MPa (pressure measurements)

Sampling rate

1 measurement/piston stroke (pump running)

1 measurement/s (pump not running)

10 measurements/s (pressure measurements)

Safety shutdown

Function

Automatic shutdown when upper and lower

pressure limits violated

Maximum pressure limit

adjustable between 0.1...25.0 MPa (1...250 bar)

Response time: 1 pump cycle

Minimum pressure limit

adjustable between 0.1 ... 25.0 MPa (1...250 bar),

inactive at 0 MPa

Response time: 5 pump cycles

Pump head

Pump head volumes Main

piston: 40

µ

L

Priming piston:

20

µ

L

Pump displacement

volumes

Main piston:

28.5

µ

L

Priming piston:

14.25

µ

L

Length of stroke

Main piston:

3.6 mm

Priming piston:

1.8 mm