Metrohm 766 IC Sample Processor - Manual (Page 90)

4.6 Standard methods
766 IC Sample Processor
85
7 CTL:Rm: STEP MSM 753
8 PUMP 1.1 : 150 s
9 CTL:Rm: ZERO 1
10 CTL:Rm: INJECT A 1
11 SAMPLE: + 1
12 MOVE 1 : sample
13 PUMP 1.1 : 5 s
14 LIFT: 1 : work mm
15 CTL:Rm: ******0*010***
16 CTL:Rm: INIT 732
17 PUMP 1.1 : 150 s
18 CTL:Rm: ******0*011***
19 CTL:Rm: INIT 732
20 CTL:Rm: ******1*000***
21 CTL:Rm: INIT 732
22 SAMPLE: + 1
>final sequence
>changer settings
rack number 0
lift rate 1 12 mm/s
shift rate 20
>manual stop
CTL Rmt: **************
CTL RS232:
------------ − Switch 753 suppressor module to next position
− Fill sample loop A with sample during 150 s
− Trigger autozero at 732/1 IC Detector
− Switch injection valve A at 733 to "Inject"
− Raise sample position by 1
− Move needle to sample position
− Aspirate air into the transfer tubing during 5 s
− Place lift with needle to working position
− Switch injection valve B at 733 to "Fill"
− Initialize remote lines at 732/1 and 732/2
− Fill sample loop B with sample during 150 s
− Trigger autozero at 732/2 IC Detector
− Initialize remote lines at 732/1 and 732/2
− Switch injection valve B at 733 to "Inject"
− Initialize remote lines at 732/1 and 732/2
− Raise sample position by 1
− —— Settings for changer functions ——
− —— Reaction to manual stop ———
Settings in the «IC Metrodata» program
1. Definition of anion method for channel 1 (analysis time, start pa-
rameters for IC instruments 732, 733 and 709, etc.), additional asso-
ciation of this method with the following time program for the 732/1
IC Detector:
Method / Equipment / Setup / Program / Text:
0.0 Puls_766_set Set remote line 3 at 732/1 to 1 (s. below)
0.1 Puls_766_reset Set remote line 3 at 732/1 to 0 (s. below)
0.2 Flag end Program end
Method / Equipment / Setup / Program / Remote configuration:
Puls_766_set = **1***** Set remote line 3 at 732/1 to 1
Puls_766_reset = **0***** Set remote line 3 at 732/1 to 0
Method / Equipment:
Start with method
2. Definition of cation method for channel 2 (analysis time, start pa-
rameters for IC instruments 732, 733 and 709, etc.). The analysis
time Duration must be shorter than the analysis time for the anion
method.
Procedure at program start
1. Create queue with cation method for channel 2 in the program «IC
Metrodata» and start it.
2. Start 766 IC Sample Processor with .
3. Create queue with anion method for channel 1 in the program «IC
Metrodata» and start it.