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Instrument equipment, O_3639 – BUCHI DuMaster D-480 User Manual

Page 51

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Operation Manual D-480

©BÜCH Labortechnik AG

4 - Understanding the instrument and planning its use

51

Instrument equipment

Combustion tube filling

The following picture shows the fillings and filling heights of the combustion tube:

Legend:

1 Ash crucible
2 Corundum balls (3 mm)
3 80 g CuO + 20 g Corundum balls (110 mm)
4 Corundum balls (10 mm)
5 Wire mesh ronde (22 mm)
6 Spacer

Working temperature 950 °C

Reduction tube filling

The following picture shows the fillings and filling heights of the reduction tube:

Legend:

1 Silver wool
2 Copper (20 mm)
3 CuO (50 mm)
4 10 x tungsten á 20 g
5 Corundum balls (55 mm)
6 Wire mesh ronde (22 mm)
7 Plug

Working temperature 815 °C