BUCHI PrepChrom C-700 - Manual (Page 4)

Table of contents BÜCHI Labortechnik AG
iv PrepChrom C­700
4.4.4 Racks and glass tubes overview ................................................................................................. 30
4.4.5 Synoptic....................................................................................................................................... 31
4.4.6 Stop modes ................................................................................................................................. 32
4.4.7 Collection..................................................................................................................................... 33
4.5 Optional accessories .............................................................................................................................. 34
4.5.1 Switching valve............................................................................................................................ 34
4.5.2 Back flush valve........................................................................................................................... 35
4.5.3 Purge valve.................................................................................................................................. 36
4.5.4 Fume enclosure........................................................................................................................... 37
5 Installation ..................................................................................................................................................... 39
5.1 Modules, assembly ................................................................................................................................. 39
5.2 Tubing, installation.................................................................................................................................. 41
5.2.1 6­way electrical valve, overview .................................................................................................. 41
5.2.2 Tubing general, installation.......................................................................................................... 41
5.2.3 Tubing Flash/prep column, installation ........................................................................................ 43
5.2.4 Tubing prep HPLC column, installation ....................................................................................... 44
5.3 Electrical, connection.............................................................................................................................. 45
5.3.1 Communication and power supply, connection ........................................................................... 45
5.3.2 External devices, connection....................................................................................................... 46
5.4 Rack and glass tubes, installation .......................................................................................................... 46
5.5 Column, preparation ............................................................................................................................... 47
5.5.1 Flash/prep column, preparation................................................................................................... 47
5.5.2 Dry load column, preparation ...................................................................................................... 48
5.5.3 Prep HPLC column, installation................................................................................................... 48
5.6 Mixing chamber volume, adjustment ...................................................................................................... 49
5.7 Software, setup....................................................................................................................................... 50
5.7.1 System configuration, setup ........................................................................................................ 50
5.7.2 User profile .................................................................................................................................. 53
5.7.3 Bottle, setup................................................................................................................................. 60
5.7.4 Column, setup ............................................................................................................................. 60
5.7.5 Rack, setup.................................................................................................................................. 61
5.7.6 Needle, offset .............................................................................................................................. 62
5.7.7 Solvent, setup.............................................................................................................................. 63
5.7.8 User management, setup ............................................................................................................ 63
5.7.9 Language, change....................................................................................................................... 64
5.7.10 Air purge, activation/deactivation................................................................................................. 64
5.7.11 Detection step, activation/deactivation ........................................................................................ 65
5.7.12 Collection step, activation/deactivation........................................................................................ 65
5.7.13 Automatic gradient optimization, activation/deactivation ............................................................. 66
5.7.14 Switching valve activation/deactivation ....................................................................................... 66
5.7.15 Back flush activation/deactivation................................................................................................ 68
5.8 System fixation (earthquake) .................................................................................................................. 70
6 Operation ....................................................................................................................................................... 71
6.1 Switch on the system.............................................................................................................................. 71
6.2 Switch off the system.............................................................................................................................. 71
6.3 Create a quick manual method............................................................................................................... 72
6.4 Create a new method ............................................................................................................................. 75
6.5 Equilibration and injection modes ........................................................................................................... 81
6.6 Make a liquid injection ............................................................................................................................ 81
6.7 Automatic method TLC, setup ................................................................................................................ 82
6.8 Purge ...................................................................................................................................................... 85
6.9 Air purge ................................................................................................................................................. 85
6.10 Data storage ........................................................................................................................................... 86