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2 attaching the tubing – Metrohm 789 Robotic Sample Processor XL User Manual

Page 49

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2.4 Connecting up accessories

Metrohm Sample Processor, Installation

41

Aspiration tip

In the macro titration head the M8 aspiration tip (6.1543.170) is placed

in a vertical opening (SGJ9). In the micro titration head a vertical open-

ing is also used. The tip is connected with a piece of PTFE tubing

(6.1805.510) and a 6.1820.030 Screw connector to Pump 2 (marking on

valve ' ').

Rinsing process

In an ideal rinsing process (with two pumps) the sample solution is first

aspirated off. The electrode is then rinsed in an empty beaker and the

rinsing solution is aspirated off at the same time. A short overrun of the

aspiration pump ensures that the sample vessel (or titration cell) is

emptied completely.

Sequence:

PUMP 1.2 : 10 s

PUMP 1.* : 3 s

PUMP 1.2 : 3 s

Chemical resistance

The pump heads of the membrane pumps, the connection nipples and

the union nuts are made of PVDF. PVDF is resistant to many chemicals.

The following should not be used: acetone, acetic anhydride or di-

methylformamide (DMF). The membrane, the valve disks and valve

components are made of PTFE and are resistant to almost all chemi-

cals.

If your sample contains solids (e.g. silver chloride) or sticky substances

then, instead of the membrane pump built into the Sample Processor,

you should use the 772 Pump Unit.

The polyethylene canisters (6.1621.000) used as rinsing or waste canis-

ters are (only) suitable for aqueous solutions.

2.4.2 Attaching the tubing

Fig. 18 Attaching the tubing

For attaching the tubing the individual

chain links can be opened with a

screwdriver or similar object.

Mind the markings on the chain links.

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