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Metrohm 789 Robotic Sample Processor XL User Manual

Page 141

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6.2 Standard methods

Metrohm Sample Processor, Annex

133

9 MOVE 1 : sample

10 LIFT: 1 : work mm

11 DOS: 1.1 : -0.5 mL

12 WAIT: pause 10 s

13 DOS: 1.2 : port mL

14 MOVE 1 : ext.1

15 SCN:Rm : Cond ok

16 WAIT: pause 60 s

17 SCN:Rm : Cond ok

18 CTL:Rm: START device1

19 LIFT: 1 : work mm

20 DOS: 1.1 : endVol mL

21 DOS: 1.1 : compen mL

22 MOVE 1 : spec.1

23 LIFT: 1 : work mm

24 SCN:Rm : Cond ok

>final sequence

1 CTL:Rm: ************1*

2 WAIT: pause 1 s

3 CTL:Rm: INIT

>changer settings

rack name: *

lift rate T1 25 mm/s

lift rate T2 25 mm/s

shift rate 20°/s

shift direction: auto

swing rate T1 55°/s

swing rate T2 55°/s

on beaker error: MOVE

>stirring rates

>Dosing unit def.

>timeout settings

SCAN timeout: OFF min

on SCAN timeout: error

>manual stop

CTL Rmt: STOP device*

CTL RS232:

PUMP: cont.

STIR T1: cont.

STIR T2: cont.

STIR MSB1: OFF

STIR MSB2: cont.

STIR MSB3: cont.

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- Move to sample beaker

- Pierce sample vial

- Aspirate sample volume

- Wait for pressure equilibration

- Close Port 1

- Move to KF cell

- Wait for conditioning

- Stabilization of "Cond." condition

- Wait for conditioning

- Start titration

- Pierce KF cell

- Eject sample volume

- Eliminate slack

- Move to parking position

- Move lift to work height

- Wait for end of titration

- Stop titrator

- Wait 1 second for stop impulse

- Initialize Remote interface
Changer settings

Stirring rates
Settings for dosing device

Actions after manual stop
- Stop titrator

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