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3 operating tutorial, 1 requirements – Metrohm 790 Personal IC User Manual

Page 60

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3.1 Requirements

790 Personal IC

51

3 Operating

tutorial


This section introduces you to the operation of the 790 Personal IC by

means of a brief operating tutorial which describes the basic operat-

ing steps needed for the recording of an ion chromatogram using one

of the system files supplied.
The determination of the cationic content of a drinking water sample

with the METROSEP Cation 1-2 column is used as an illustrative

example. Please note that the steps and parameter settings de-

scribed apply only to this example. If you use a different separating

column and system file, the procedures described in the tutorial must

be modified appropriately.
For further explanations of the operation, please refer to section 4.





3.1 Requirements

For the determination of cations in drinking water described in this tuto-

rial, the following instruments, accessories and solutions are required:

2.790.0010 Personal IC

(or 2.790.0020 Personal IC without connection

of suppressor module)

6.1825.230 Sample loop (10 µµµµL, PEEK)

already integrated in the 2.790.0010 Personal IC

6.1006.100 IC cation column

METROSEP Cation 1-2 (6.1010.000)

Eluent

4 mmol/L tartaric acid / 1 mmol/L dipicolinic acid in dist. H

2

O

flow: 1.0 mL/min

Standard

Standard solution with 1 mg/L Li

+

, 5 mg/L Na

+

, 5 mg/L NH

4

+

10 mg/L K

+

, 10 mg/L Ca

2+

, 10 mg/L Mg

2+

(in dist. H

2

O)