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4 high-pressure pump, 5 peristaltic pump – Metrohm 790 Personal IC User Manual

Page 181

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6 Appendix

790 Personal IC

172

6.1.4 High-pressure

pump

Type

Serial dual piston pump with two valves

Pump capacity

Flow range

0.20...2.5 mL/min

Maximum error

< ± 2 % of set value

Flow constancy

< 0.5 % of set value

Reproducibility of eluent

flow

typ. better than ± 0.1 %

Pressure measurement

Pressure range

0...25.0 MPa (0...250 bar)

Residual pulsation

< 10 % (at 1 mL/min water and 10 MPa pressure,

without pulsation dampener)

Measurement principle

Piezoresistive measurement

Response time: 3 ms

Measurement volume: ca. 50 µL

Maximum error

± 3 % of set value

Resolution

0.1 MPa (conductivity measurements)

Sampling rate

1 measurement/piston stroke (pump running)

1 measurement/s (pump not running)

Safety shutdown

Function

Automatic shutdown when upper and lower

pressure limits violated

Maximum pressure limit

adjustable between 0.1...25.0 MPa (1...250 bar)

Response time: 1 pump cycle

Minimum pressure limit

adjustable between 0.1 ... 25.0 MPa (1...250 bar),

inactive at 0 MPa

Response time: 5 pump cycles

Pump head

Pump head volumes Main

piston: 40

µL

Priming piston:

20 µL

Pump displacement

volumes

Main piston:

28.5 µL

Priming piston:

14.25 µL

Length of stroke

Main piston:

3.6 mm

Priming piston:

1.8 mm

6.1.5 Peristaltic

pump

Type

2-channel peristaltic pump

Pump capacity

Rotational speed

20 U/min at 50 Hz

24 U/min at 60 Hz

Flow range

0.5…0.6 mL/min with 6.1826.060 Pump tubing

Maximum error

± 5 %

Maximum pressure

0.4 MPa (4 bar)

Pumpable liquids

Clear liquids with no solid contents

Pump tubing material

PP (polypropylene)