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Chromium, testab – LaMotte SMART Spectro Spectrophotometer User Manual

Page 116

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CHROMIUM, TESTAB

DIPHENYLCARBOHYDRAZIDE TESTAB METHOD

CODE 3697-SC

QUANTITY

CONTENTS

CODE

50

*Chromium Spectrophotometric Grade Tablets

*3889A-H

1

Tablet Crusher

0175

*WARNING: Reagents marked with an * are considered to be potential health

hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents

go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail,

phone or fax.

Chromium is one of a class of heavy metals found in the bottom mud of polluted

bodies of water. It is considered to be a toxic chemical. Chromium will become

concentrated in some shellfi sh, endangering the health of the human or animal

that consumes them. Chromium may be present in water containing waste from

industries such as metal plating. If more than 0.5 ppm chromium is present, it is

evidence of contamination from untreated or incompletely treated industrial waste.

APPLICATION:

Drinking, surface, and saline waters; domestic and

industrial wastewaters.

RANGE:

0.00–1.00 ppm Chromium

MDL:

0.03 ppm

METHOD:

Hexavalent chromium reacts with 1,5

diphenylcarbohydrazide under acidic conditions to

form a red-purple color in proportion to the amount

of chromium present.

SAMPLE HANDLING &

PRESERVATION:

Analysis for chromium should be made as quickly

as possible. Storage in plastic or glass containers

may result in low results.

INTERFERENCES:

High concentrations of mercurous and mercuric

ions may impart a blue color to the chromium

determination. Iron and vanadium in concentrations

above 1 ppm may result in a yellow color.

SMART Spectro Test Procedures 2.11

CHROMIUM, TesTab

Test P

rocedures