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The 833 ic liquid handling sample preparation unit – Metrohm 833 IC Liquid Handling Unit User Manual

Page 47

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6.1 Connection to modular IC system for neutralization

833 IC Liquid Handling Unit / Instructions for Use 8.833.1003

39


36 Inlet capillary for sample

37 Inlet capillary for acid

38 Outlet capillary for acid

39 Outlet capillary for H

2

O

40 Inlet capillary for H

2

O

41 Outlet capillary for sample


Fig. 13:

Connections at sample preparation module of the 833 IC Liquid
Handling Sample Preparation Unit

1 Insert sample preparation module

Place sample preparation module 33 inside the chamber on

the floor.

2 Connect sample preparation module

Remove plastic stoppers from the rear panel openings 18 of

the 820 IC Separation Center and lead cable 35 mounted on

sample preparation module 33 back through this opening.

Connect cable 35 to connection 13 “Module” of the 833 IC

Liquid Handling Unit (see Fig. 2).

3 Connect sample feed to sample preparation

module (Sample Preparation connection 1)

Connect inlet capillary 36 (marked with “Sample in”) at the

sample preparation module connection 34 (see Fig. 13) to

connection “5” of injection valve B using a 6.2744.010

compression fitting.

4 Connect sample preparation module to valve A

(enrichment column) (Sample Preparation

connection 1)

Connect outlet capillary (marked “Sample out”) at sample

preparation module connection 34 (see Fig. 13) to

connection “1” of injection valve A using a 6.2744.010

compression fitting.

When making the further connections to injection valve A

make sure that the ”Inject” setting of the enrichment column

is rinsed in the reverse direction to the “Fill” setting.

Sample in

H

2

O

Sample out

Waste

Waste

Regenerant

1

3

2

39

36

37

38

40

41