10 appendix – Metrohm 833 IC Liquid Handling Unit User Manual
Page 120
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10 Appendix
833 IC Liquid Handling Unit / Gebrauchsanweisung 8.833.1001
112
Contents................................................... I
Correct connection .........................35, 49
Coupling
6.2744.040 ..................................45, 98
Coupling 18
Assembly ..........................................20
Figure ....................................19, 58, 71
Ordering designation...........95, 97, 98,
100, 102
Coupling 21
Assembly ........................60, 61, 70, 72
Figure ....................................19, 58, 71
Ordering designation..........96, 97, 100
Coupling 6.2620.060 ............................33
Coupling 71
Mounting .....................................29, 33
D
Danger .................................................... 9
Declaration of Conformity...................109
Degassed..............................................66
...............................................25
Delivery rate
Pump.................................................21
Determinations with dialysis .................66
Determining the dialysis time ...............64
Determining the rinsing time ................63
Determining the transfer time ...............63
Dialysis
Connect injection valve ....................61
Connections to Suppressor..............57
Mount aspiration capillary ..........59, 60
Preparation of Separation Center.....57
With suppression
Electrical connection ..................53
Settings in IC Net........................55
Without suppression
Electrical connection ..................52
Settings in IC Net........................54
Dialysis cell ...........................................50
Connection........................................58
Acceptor solution .......................61
Sample solution..........................60
Dialysis cell 42
Assembly ..........................................56
Clean.................................................56
Connection to IC system ............59, 89
Dismantle ..........................................89
Figure ..........................................50, 58
Insert membrane...............................56
Ordering designation........................99
Prepare..............................................56
Technical data ..................................94
Dialysis cell construction ......................50
Dialysis membrane ...............................64
Dialysis membrane 45
Conditioning................................62, 89
Figure ................................................50
Insert .................................................56
Ordering designation................99, 106
Prepare..............................................56
Replace.............................................89
Treatment..........................................88
Dialysis procedure ................................66
Dialysis system shut down ...................67
Dialysis time....................................64, 78
Dialysis with ..........................................51
Dialyze and measure standard ............65
Dimensions ...........................................93
Discharge capillary 23
Figure ..........................................19, 81
E
Electrical connection ................ 44, 47, 52
833 LH Sample Preparation Unit ..... 41
Electrical connections .......................... 37
Electrical safety..................................... 10
Electromagnetic compatibility.............. 93
Electrostatic charges............................ 10
Emission ............................................... 93
EMV....................................................... 93
ENABLED
.............................................. 25
EU-Konformitätserklärung.................. 109
F
Feedthrough 14
Mounting of suppressor inlet
capillary............................................. 29
Figures
list....................................................... IV
Filling 2 sample loops .......................... 73
Filter membrane
Replace............................................. 90
Selection ........................................... 75
Filter membrane 72
Ordering designation.............. 101, 106
Filter unit PEEK 22
Assembly .......................................... 81
Figure................................................ 19
Filter change..................................... 81
Ordering designation............ 96, 97, 98
Filter unit PEEK 6.2821.120
Assembly .......................................... 81
Connection to 833 Pump Unit.......... 29
Connector ......................................... 81
Figure................................................ 81
Filter .................................................. 81
Housing ............................................ 81
Filtration ................................................ 74
Choice of filter membrane................ 75
Filter working life............................... 74
Membrane blockage ........................ 74
Pore size ........................................... 74
Recovery rate.................................... 74
Sample type...................................... 74
Filtration cell.......................................... 68
Close down....................................... 73
Connection ....................................... 70
Filtration cell 66
Connect to IC system....................... 90
Connection to IC system.................. 70
Figure................................................ 71
Filtration membrane
6.2714.020 ........................................ 74
Handling ........................................... 90
Filtration membrane 72
Figure................................................ 68
Insert ................................................. 69
Prepare ............................................. 69
Flow diagram for dialysis ..................... 51
Flow direction ................................. 35, 49
Front panel.............................................. 6
Fuse ................................................ 12, 13
Fuse holder 11
Figure............................................ 7, 13
Fuses .................................................... 91
G
General safety rules.............................. 10
GLP ............................................. 107, 110
GMP.................................................... 110
Grounding....................................... 10, 13
H
H
2
O ..................................... 29, 34, 40, 46
H
2
SO
4
.............................................. 29, 33
Handling
Sample preparation module ............ 49
Suppressor module.......................... 35
Holding clip 6
Assembly pump tubing.................... 20
Figure.................................................. 6
Tubing cassette assembly ............... 80
Holding pin 2
Assembly tubing cassette................ 20
Figure.................................................. 6
Tubing cassette assembly ............... 80
Housing ................................................ 93
I
Icon
833 IC Dialysis Unit .......................... 23
833 IC Liquid Handling Unit............. 23
833 IC Pump Unit ............................. 23
833 IC Sample Preparation Unit ...... 23
833 IC Suppressor Unit.................... 23
833 IC Ultrafiltration Unit .................. 23
Immunity ............................................... 93
Inadequate supply.......................... 76, 77
Information.............................................. 9
Information about these Instructions
for Use .................................................... 8
Injection ................................................ 51
Injection valve 56
Figure................................................ 58
Inlet 50
Capillary connection......................... 61
Figure................................................ 50
Inlet 51
Capillary connection......................... 60
Figure................................................ 50
Inlet 73
Figure................................................ 68
Inlet capillary 27
Connection ....................................... 33
Inlet capillary 28
Connection ....................................... 33
Inlet capillary 31
Connection ....................................... 34
Inlet capillary 36
Connection ................................. 39, 45
Figure................................................ 39
Inlet capillary 37
Connection ................................. 40, 46
Inlet capillary 40
Connection ................................. 40, 46
Figure................................................ 39
Inline filter
6.2821.120........................................ 27
Installation............................................. 11
Instructions for Use .... 95, 96, 97, 98, 100
Instrument care .................................... 79
Instrument checks................................ 11
Instrument description ........................... 1
Instrument setup .................................. 11
Introduction............................................. 1
IQ ........................................................ 107