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10 appendix – Metrohm 833 IC Liquid Handling Unit User Manual

Page 120

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10 Appendix

833 IC Liquid Handling Unit / Gebrauchsanweisung 8.833.1001

112

Contents................................................... I
Correct connection .........................35, 49
Coupling

6.2744.040 ..................................45, 98

Coupling 18

Assembly ..........................................20

Figure ....................................19, 58, 71

Ordering designation...........95, 97, 98,

100, 102

Coupling 21

Assembly ........................60, 61, 70, 72

Figure ....................................19, 58, 71

Ordering designation..........96, 97, 100

Coupling 6.2620.060 ............................33
Coupling 71

Mounting .....................................29, 33

D

Danger .................................................... 9
Declaration of Conformity...................109
Degassed..............................................66

...............................................25

Delivery rate

Pump.................................................21

Determinations with dialysis .................66
Determining the dialysis time ...............64
Determining the rinsing time ................63
Determining the transfer time ...............63
Dialysis

Connect injection valve ....................61

Connections to Suppressor..............57

Mount aspiration capillary ..........59, 60

Preparation of Separation Center.....57

With suppression

Electrical connection ..................53

Settings in IC Net........................55

Without suppression

Electrical connection ..................52

Settings in IC Net........................54

Dialysis cell ...........................................50

Connection........................................58

Acceptor solution .......................61

Sample solution..........................60

Dialysis cell 42

Assembly ..........................................56

Clean.................................................56

Connection to IC system ............59, 89

Dismantle ..........................................89

Figure ..........................................50, 58

Insert membrane...............................56

Ordering designation........................99

Prepare..............................................56

Technical data ..................................94

Dialysis cell construction ......................50
Dialysis membrane ...............................64
Dialysis membrane 45

Conditioning................................62, 89

Figure ................................................50

Insert .................................................56

Ordering designation................99, 106

Prepare..............................................56

Replace.............................................89

Treatment..........................................88

Dialysis procedure ................................66
Dialysis system shut down ...................67
Dialysis time....................................64, 78
Dialysis with ..........................................51
Dialyze and measure standard ............65
Dimensions ...........................................93
Discharge capillary 23

Figure ..........................................19, 81

E

Electrical connection ................ 44, 47, 52

833 LH Sample Preparation Unit ..... 41

Electrical connections .......................... 37
Electrical safety..................................... 10
Electromagnetic compatibility.............. 93
Electrostatic charges............................ 10
Emission ............................................... 93
EMV....................................................... 93

ENABLED

.............................................. 25

EU-Konformitätserklärung.................. 109

F

Feedthrough 14

Mounting of suppressor inlet

capillary............................................. 29

Figures

list....................................................... IV

Filling 2 sample loops .......................... 73
Filter membrane

Replace............................................. 90

Selection ........................................... 75

Filter membrane 72

Ordering designation.............. 101, 106

Filter unit PEEK 22

Assembly .......................................... 81

Figure................................................ 19

Filter change..................................... 81

Ordering designation............ 96, 97, 98

Filter unit PEEK 6.2821.120

Assembly .......................................... 81

Connection to 833 Pump Unit.......... 29

Connector ......................................... 81

Figure................................................ 81

Filter .................................................. 81

Housing ............................................ 81

Filtration ................................................ 74

Choice of filter membrane................ 75

Filter working life............................... 74

Membrane blockage ........................ 74

Pore size ........................................... 74

Recovery rate.................................... 74

Sample type...................................... 74

Filtration cell.......................................... 68

Close down....................................... 73

Connection ....................................... 70

Filtration cell 66

Connect to IC system....................... 90

Connection to IC system.................. 70

Figure................................................ 71

Filtration membrane

6.2714.020 ........................................ 74

Handling ........................................... 90

Filtration membrane 72

Figure................................................ 68

Insert ................................................. 69

Prepare ............................................. 69

Flow diagram for dialysis ..................... 51
Flow direction ................................. 35, 49
Front panel.............................................. 6
Fuse ................................................ 12, 13
Fuse holder 11

Figure............................................ 7, 13

Fuses .................................................... 91

G

General safety rules.............................. 10
GLP ............................................. 107, 110

GMP.................................................... 110
Grounding....................................... 10, 13

H

H

2

O ..................................... 29, 34, 40, 46

H

2

SO

4

.............................................. 29, 33

Handling

Sample preparation module ............ 49

Suppressor module.......................... 35

Holding clip 6

Assembly pump tubing.................... 20

Figure.................................................. 6

Tubing cassette assembly ............... 80

Holding pin 2

Assembly tubing cassette................ 20

Figure.................................................. 6

Tubing cassette assembly ............... 80

Housing ................................................ 93

I

Icon

833 IC Dialysis Unit .......................... 23

833 IC Liquid Handling Unit............. 23

833 IC Pump Unit ............................. 23

833 IC Sample Preparation Unit ...... 23

833 IC Suppressor Unit.................... 23

833 IC Ultrafiltration Unit .................. 23

Immunity ............................................... 93
Inadequate supply.......................... 76, 77
Information.............................................. 9
Information about these Instructions

for Use .................................................... 8
Injection ................................................ 51
Injection valve 56

Figure................................................ 58

Inlet 50

Capillary connection......................... 61

Figure................................................ 50

Inlet 51

Capillary connection......................... 60

Figure................................................ 50

Inlet 73

Figure................................................ 68

Inlet capillary 27

Connection ....................................... 33

Inlet capillary 28

Connection ....................................... 33

Inlet capillary 31

Connection ....................................... 34

Inlet capillary 36

Connection ................................. 39, 45

Figure................................................ 39

Inlet capillary 37

Connection ................................. 40, 46

Inlet capillary 40

Connection ................................. 40, 46

Figure................................................ 39

Inline filter

6.2821.120........................................ 27

Installation............................................. 11
Instructions for Use .... 95, 96, 97, 98, 100
Instrument care .................................... 79
Instrument checks................................ 11
Instrument description ........................... 1
Instrument setup .................................. 11
Introduction............................................. 1
IQ ........................................................ 107