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Metrohm 794 Basic Titrino User Manual

Page 41

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2.7 Parameters, key

794 Basic Titrino

37

min.rate 25.0 µl/min
**titr.






stop crit: drift
**titr.
stop drift 20 µl/min
**titr.

t(delay) 10 s
**titr.







stop time OFF s
**titr.

Minimum dosing rate (0.01...999.9 µL/min)

This parameter determines the addition rate right at the

start and the end of the titration, see also page 42.

This parameter influences the titration speed and

therefore its accuracy very strongly: A smaller min.rate

results in a slower titration.

Type of stop criteria (drift, time)

Titration stops if EP is and stop drift is reached. (1...999

µL/min)

Titration stops if there is no dosing during t(delay).

(0...999 s, INF)

sets "INF"

Switch off when the end point is reached and the set

time after the last dispensing has elapsed.

If "INF" is set, an inquiry regarding the stop time

appears.

If t(delay) is "INF"

Stop after a time (0...999999 s, OFF)

sets "OFF".

Stop after the set time after the start of the titration.

"OFF" means no stop, i.e. titration for an "infinitely" long

time.


>titration parameters

titr.direction: auto









start V: OFF
cond.




start V 0.0 ml
cond.


factor 0
cond.



dos.rate max. ml/min

**titr.



General titration parameters

Direction is set automatically (+, -, auto)

auto: The direction is set automatically by the Titrino

(sign [U

first

- EP]).

+:

Direction of higher pH, higher voltage (more

"positive"), larger currents.

- :

Direction of lower pH, lower voltage, smaller

currents.

The titration direction is fixed if two EP's are set. In this

case, an input for titration direction has no meaning.

Type of start volume (OFF, abs., rel.)

"OFF":

start volume switched off

"abs.":

absolute start volume in mL

"rel.":

relative start volume to sample size.

If "abs." is set:

Absolute start volume (0...999.99 mL)

If "rel." is set:

Factor for relative start volume (0...±999999).

Calculated as: start V (in mL) = factor∗sample size

Dosing rate for start volume

(0.01...150 mL/min, max.)

sets "max.".

The maximum rate depends on the Exchange Unit: