beautypg.com

Metrohm 844 UV/VIS Compact IC User Manual

Page 66

background image

Table of contents

5 Check for leaks

• Check all the capillaries and their connections from the high-

pressure pump to the detector block for escaping liquid. If

eluent is escaping then the corresponding compression

fitting should be tightened or a new connection should be

made.

6 Condition system

• Rinse the system with eluent until the desired stability of the

baseline is reached (normally 30…60 min; if the eluent is

changed, the establishment of the ion exchanger equilibrium

on the separating column can take longer).

• The instrument is now ready for sample determinations using

the selected system.

Pump tubings are consumable material with a lifetime which depends

on the contact pressure. This is why the tubing cartridges should be

raised completely by loosening snap-action lever on the right-hand si-

de if the pump is to remain switched off for a considerable length of

time (the set contact pressure remains unchanged).