Metrohm 844 UV/VIS Compact IC - Manual (Page 5)

Table of contents
844 UV/VIS Compact IC / Gebrauchsanweisung 8.844.1051
I
Table of contents
1 Introduction ................................................................ 1
1.1 Instrument description ................................................................................1
1.2 Parts and controls .......................................................................................3
1.2.1 Front.................................................................................................................... 3
1.2.2 Rear panel .......................................................................................................... 5
1.2.3 Interior PEEK versions ........................................................................................ 7
1.2.4 Interior Steel versions ......................................................................................... 9
1.3 Information on the Instructions for Use ...................................................11
1.3.1 Organization ..................................................................................................... 11
1.3.2 Notation and pictograms.................................................................................. 12
1.4 Safety notes ...............................................................................................13
1.4.1 Electrical safety................................................................................................. 13
1.4.2 General precautionary rules ............................................................................. 13
1.4.3 Recycling and disposal .................................................................................... 13
2 Installation ............................................................... 14
2.1 Overview ....................................................................................................14
2.1.1 Flow chart ......................................................................................................... 14
2.1.2 Connections in the 844 UV/VIS Compact IC.................................................... 15
2.2 Setting up the instrument..........................................................................20
2.2.1 Packaging......................................................................................................... 20
2.2.2 Check................................................................................................................ 20
2.2.3 Location ............................................................................................................ 21
2.3 Attaching the accessories.........................................................................21
2.3.1 Connecting the syringe and aspirating tubing................................................. 21
2.3.2 Connecting the drainage tubing for the inner compartment ........................... 21
2.3.3 Connecting PEEK capillaries............................................................................ 21
2.3.4 Connecting Steel capillaries............................................................................. 22
2.3.5 Filter unit PEEK ................................................................................................. 23
2.3.6 Filter unit Steel .................................................................................................. 24
2.4 Mains connection ......................................................................................25
2.4.1 Setting the mains voltage................................................................................. 25
2.4.2 Fuses ................................................................................................................ 26
2.4.3 Mains cable and mains connection ................................................................. 26
2.4.4 On/off switching of the instrument ................................................................... 27
2.5 Connection to PC ......................................................................................27
2.5.1 Connecting cable ............................................................................................. 27
2.5.2 Software installation.......................................................................................... 27
2.5.3 First Login ......................................................................................................... 28
2.5.4 Create a system ............................................................................................... 28
2.6 High-pressure pump .................................................................................29
2.6.1 Removing the transport security screws.......................................................... 29
2.6.2 Installing the pulsation dampener.................................................................... 29
2.6.3 Connecting the eluent bottle ............................................................................ 31
2.6.4 Deaerating the pump and rinsing the pulsation dampener............................. 32
2.7 Post column reactor ..................................................................................34
2.7.1 Preparing the peristaltic pump......................................................................... 34
2.7.2 Installation of the post column reactor............................................................. 36
2.7.3 Post column reactor tubing connections ......................................................... 37
2.7.4 Reagent bottle connection ............................................................................... 38
2.8 Columns.....................................................................................................39