2 loading samples with a vacuum syringe, 3 loading samples with an autosampler – Oritron Dionex Ion Chromatography System ICS-2100 User Manual
Page 76
ICS-2100 Ion Chromatography System
64
Doc. 065291-01 3/09
3.10.2 Loading Samples with a Vacuum Syringe
1. Disconnect the waste line from port
W (6)
of the injection valve (see
Figure 3-10
) and attach a shorter line: 25 to 30 cm (10 to 12 inches) of
PEEK or Teflon
®
tubing.
2. Place the free end of the line into the sample.
3. Verify that the injection valve is in the Load position.
4. Insert the 1 cc syringe (P/N 016388) provided in the ICS-2100 Ship
Kit (P/N 064375) into the injection port on the ICS-2100 front door
(see
) and pull out the plunger to draw the sample into the
injection valve.
5. Switch the injection valve to the Inject position (see
3.10.3 Loading Samples with an Autosampler
1. Verify that the autosampler output line is connected to port
S (5)
of the
ICS-2100 injection valve.
2. Prepare and fill the sample vials and place them in the autosampler
tray or cassette. Refer to the autosampler manual for detailed
instructions.
3. The sample loading process depends on the autosampler. Refer to the
autosampler manual for detailed instructions. In general, use one of
the following methods:
•
Include the commands for controlling sample loading in a
Chromeleon program. (If necessary, refer to the Chromeleon
Help or user manual for assistance.)
•
Enter the commands for loading the sample on the autosampler
front panel.
4. Switch the injection valve to the Inject position (see