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Appendix a - cone/plate rheometer set-up – Brookfield DV-III Ultra Rheometer User Manual

Page 95

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Brookfield Engineering Laboratories, Inc.

Page 95

Manual No. M/98-211-B0104

Brookfield Engineering Laboratories, Inc.

Page 95

Manual No. M98-211-E0912

APPENDIX A - Cone/Plate Rheometer Set-Up

This Cone/Plate version of the DV-III Ultra uses the same operating instruction procedures as described

in this manual. However, the “gap” between the cone and the plate must be verified/adjusted before

measurements are made. This is done by moving the plate (built into the sample cup) up towards the

cone until the pin in the center of the cone touches the surface of the plate, and then by separating

(lowering) the plate 0.0005 inch (0.013mm).
Programmable DV-III Ultra Cone/Plate Viscometers, S/N 50969 and higher, have an Electronic Gap

Setting feature. This feature enables the user to easily find the 0.0005 inch gap setting that was established

at Brookfield prior to shipment.
The following information explains how to set the Electronic Gap and verify calibration of the DV-III

Ultra Viscometer. Acceptable operating temperature range is 0ºC to 100ºC. Be careful about condensation

and the possible formation of ice crystals when approaching 0ºC. Setting the gap should be accomplished

at the same temperature that you intent to use for testing your material.

A.1 ELELECTRONIC GAP SETTING FEATURES

TOGGLE SWITCH

allows you to enable/disable the Electronic Gap Setting Feature: left position is OFF

(disabled), right position is ON (enabled).

PILOT LIGHT

is the red (LED) light; when illuminated, it means the Electronic Setting Function is

sensing (enabled).

CONTACT LIGHT

is the yellow (LED) light; when it first turns on, the “hit point” has been found.

SLIDING REFERENCE MARKER

is used after finding the “hit point;” it is the reference for establishing

the 0.0005 inch gap.

MICROMETER ADJUSTMENT RING

is used to move the cup up or down in relation to the cone spindle.

Turning the ring left (clockwise) lowers the cup; turning it right (counterclockwise) raises the cup.

Each line on the ring represents one scale division and is equivalent to 0.0005 inch movement of the

plate relative to the cone.

Figure

A-1

Pilot Light

(red)

Toggle Swtich

Contact Light

(yellow)

Sliding Reference

Marker

Micrometer

Adjustment Ring