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Metrohm 873 Biodiesel Rancimat Manual User Manual

Page 6

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Table of contents

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IV

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873 Biodiesel Rancimat

4.1.6

Context-sensitive menus ........................................................ 31

4.1.7

Mouse functions .................................................................... 31

4.1.8

Help ...................................................................................... 32

4.2

Instrument and Program Settings ..................................... 33

4.2.1

Establishing the instrument communication ........................... 33

4.2.2

Managing access rights ......................................................... 34

4.2.3

Timer ..................................................................................... 37

4.2.4

Gas flow control .................................................................... 39

4.2.5

Recording the temperature .................................................... 40

4.2.6

Optimizing program and database ......................................... 41

4.3

Program information ......................................................... 42

4.3.1

Instrument information .......................................................... 42

4.3.2

Status overview ..................................................................... 44

4.3.3

Displaying, filtering and deleting event overview .................... 45

4.4

Calibration functions .......................................................... 48

4.4.1

Determining cell constants ..................................................... 48

4.4.2

Determining Delta T .............................................................. 50

4.5

Methods .............................................................................. 55

4.5.1

Managing methods ............................................................... 55

4.5.2

Parameter description ............................................................ 60

4.6

Determinations ................................................................... 75

4.6.1

Preparing the instrument and the accessories ......................... 76

4.6.2

Preparing the determination .................................................. 77

4.6.3

Starting the determination ..................................................... 79

4.6.4

Cleaning the instrument and accessories ................................ 80

4.6.5

Adjusting the method parameters during the determina-
tion .......................................................................................
81

4.6.6

Stopping the determination manually .................................... 81

4.6.7

Status of the live curve ........................................................... 82

4.7

Results ................................................................................. 83

4.7.1

Determination overview ......................................................... 83

4.7.2

Determination and method data ............................................ 99

4.7.3

Graph and reevaluation ....................................................... 108

4.7.4

Extrapolation ....................................................................... 113

4.7.5

Recalculating a determination .............................................. 117

4.7.6

Printing and exporting data ................................................. 124

4.7.7

Program settings ................................................................. 131

4.7.8

Arranging windows ............................................................. 137

4.8

GLP functions .................................................................... 138

4.8.1

General information on GLP and validation .......................... 138

4.8.2

GLP monitoring ................................................................... 138

4.8.3

GLP status ........................................................................... 140

4.8.4

Carrying out GLP tests ......................................................... 141

4.8.5

GLP results .......................................................................... 151