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Brookfield DV3T Rheometer User Manual

Page 35

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Brookfield Engineering Labs., Inc.

Page 35

Manual No. M13-2100

TIP: An End Condition of zero Time can be useful when measuring a new material.

During the test, the speed can be changed without ending and then rerunning

the test (see Section III.10). This method can allow you to quickly evaluate the

spindle selection to determine the best speeds for testing.

# of Points: The test will complete when the specified number of data points has been collected.

Data is collected according to the Data Collection setting (see Section III.6). The

range of data points is: 1 – 9,999.

# of Revolutions: The test will complete when the specified number of revolutions of the spindle

has occurred. Data is collected according to the Data Collection setting (see

Section III.6). The range for number of revolutions is: 1 – 9,999.

Torque: The test will complete when the specified Torque value is measured. Data is collected

according to the Data Collection setting (see Section III.6). The range of values for

the measured Torque is: -10.0 – 100.0.

Viscosity: The test will complete when the specified Viscosity value is measured. Data is

collected according to the Data Collection setting (see Section III.6). The range of

measured Viscosity is 0 – 10,000,000,000 cP.

Note: The Viscosity End Condition should be selected in consideration of the Range

provided by the spindle and speed selected. Check the Range value by selecting

Spindle in Configure Viscosity Test. If you choose a Viscosity End Condition

greater than the Range of the spindle and speed settings, then the value shown in

the End Condition field will be EEEE. In this case, the end condition will never be

achieved.

Temperature: The test will complete when the specified Temperature value is measured to

within the indicated Tolerance. The Tolerance specifies how close the measured

temperature should be to the specified temperature value to consider the target

reached. Temperature is measured through the use of a connected Brookfield

temperature probe (DVP-94Y, CPA-44ZPY cup, SC4-XXRPY chamber). Data

is collected according to the Data Collection setting (see Section III.6).

Temperature: -100 – 300 C

Tolerance: 0.0 – 9.9 C

TIP: A small tolerance value will require a much longer time to reach the

End Condition.

TIP: Consider using a larger Tolerance value for the End Condition and

then use a second step for thermal equilibrium (End Condition Time).

This two step method can reduce the variability in test time caused by

variations in temperature sensors.

III.9 Additional Test Parameters

The Configure Viscosity Test screen includes a More/Less Bar. When pressed, the More Bar will

present several additional Test Parameters including: QC Limits, Instructions, Reports, and Density.

These parameters are always available and active regardless of the position of the More / Less Bar.

QC Limits: Select an acceptable range for measurement results. The range may be defined

by Viscosity, Torque, Time, Temperature, or Shear Stress. The possible range for

Viscosity and Shear Stress will be defined by the spindle and speed selected. QC

Limits are a visual and audible signal to the operator during the test. The data set

does not include an indication of QC Limits violation.