beautypg.com

Metrohm 714 IC Metrodata User Manual

Page 29

background image

3.3 Use of existing methods

IC Metrodata for Win95

23

Preparations

Insert separating column in IC system and condition it.

Prepare standards and sample.

Load standard method and run

Click on

or select

Load method and run

from the

Acquire

menu.

Select the desired method (e.g.

dual1sup.mtw

) in the

File Open

win-

dow and click the

OK

button. The window

Start Run

appears.

Enter a name as

Ident

to characterize the standard (max. 14 char-

acters, e.g. "standard").

Change the analysis time

Duration

if required.

Enter more parameters to characterize sample and acquirement

conditions if required.

Click the

OK

button.

The window for the on-line display of the chromatogram opens.

The window title line contains sample name, method and run num-

ber (e.g.

standard (dual1sup.mtw)01.run

). The status display below

shows the message

Waiting

.

Set injection valve at 733 IC Separation Center to "FILL" (manually

or by program) and fill sample loop with standard.

Set injection valve at 733 IC Separation Center to "INJECT" (manu-

ally or by program). The data acquisition is started automatically

and stopped as soon as the analysis time has passed. As the

Re-

start method

option is switched on in the method, the chroma-

togram is saved automatically and deleted in the chromatogram

window.