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2 developing a new method – Metrohm 714 IC Metrodata User Manual

Page 16

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3 Learning by doing

IC Metrodata for Win95

10

3.2 Developing a new method

This section describes the procedure how to develop a new, user-

specific method based on a standard method.

Preparation

Insert separating column in IC system and condition it.

Prepare standards and sample.

Load standard method and run

Click on

or select

Load method and run

from the

Acquire

menu.

Select the file

1m732b1.mtw

in the

File Open

window and click the

OK

button.

In the

Start Run

window, enter a sample name as

Ident

to character-

ize the chromatogram (max. 14 characters, e.g. "standard").

Enter the estimated analysis time as

Duration

.

Select the tabs

Sample

,

Eluent

,

Measure

and

Processing

to enter

more parameters to characterize sample and acquirement condi-

tions if required.

Click the

OK

button.

The window for the on-line display of the chromatogram opens.

The window title line contains sample name, method and run num-

ber (e.g.

standard (1m732b1.mtw)01.run

). The status display below

shows the message

Waiting

.